FINALInvestigation of Geophysical AnomalyGambell, St. Lawrence Island, AlaskaContract No . Delivery Order No .DACA85-93-D-001 1 0016Modification No . P0003December 1997Prepared for :Department of the ArmyUnited States Army Engineer District, AlaskaCorps of EngineersP.O. Box 898Anchorage, Alaska 99506-0898Prepared by :Montgomery Watson4100 Spenard RoadAnchorage, Alaska 99517VOL 1 OF 2F 1 OAK069602 03 .10 0500_p200-1 fTable of Contents1 . INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . .. .. .. .... .......... ...... ... . . ....... . ...... . ............................................... .1-11 .1 Previous Documents . . . . . . .. .. .. .. .. .. .. ...................................... . ........... . .............................. .1-11 .2 Site Description . . . . . . . . . . . . . . . .. .. .. .... .. .. ............................................ . .................................. .1-21 .3 Background Information . .. .. .. .... .. .. .................................. . . . .... . . . . ... . ... . .... . . . . . . . . . . . . . . . . . . . . . . ..1-21 .4 Project Objective . . . . . . . . . . . . . . . . . .. .. .... .. .. .............................. . ... . . . ..... . .................................. .1-32 . FIELD OBSERVATIONS AND INVESTIGATION RESULTS ............ . .................... . ....... . .2-12.1 Training Of Local Personnel . .. .. .. .. .. .. ........................... ... . .. . . . . .... .. . ..... ...... ... . ... ..... ........ .2-12.2 Emergency Water Treatment System ........................................................................... .2-12 .3 Public Meeting . . . . . . . . . . .. . . . . .. .. .. .... .. .................................. . .............................................. .2-22 .4 Anomaly Investigation .. .. .. ............................ . ............... . ................................. ............. . 2-22 .4 .1 Investigation at Anomaly #1 ....... . . . ... . . . ............... . ...................................... . . . . .. .2-22 .4.2 Investigation at Anomaly #2 ... .. . . .. . .. .. .. .. .. .. ... . .. .. .. .. .. .. .. .. ... . .. .. .. .... ... . .. .............. .2-32.5 Supplemental Metal Detection Scanning . . . . . . . . . . . ... . ....... . . . . . . . . . . . . . ... . . . . . ..................... . .... .2-32.6 Archaeologist Supervision .................. . .. .. .. .. .. .. .. .. .. .. .. .. . . . . . . . . .. .. .. .. .. .. .. .. .. .. .. .. .. .. ... . .. .. .. .. .2-32.7 Sampling . . . . . . . . . . . . . . . . .. .. .. .. ...................... . .. .. .. .. .. .. .. .. .. .. .. .. .. .. . . .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ... . .. . . .. .. . 2-42 .7 .1 Soil and Wipe Sampling ............ . .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ....... . .. .. .. .. .. . . . . .. .2-42 .7.2 Groundwater Sampling and Monitoring Well Decommissioning . . . . . . . . . . . . . . . . . . . . .2-42 .7.3 Data Review .. .. ........................ . .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. . . .. .. .. .. .. .. .. ......... . .. .. .. .. .... . 2-52.8 Removal Of Transformers At Site 4/Area 4d . .. .. .. .. .. .. .. .. .. .. .. . . .. . . .. .. .. .. .. .. .. ... . .. ... . .. .. . . .. .. . 2-52.9 Collection And Packaging Of Associated Debris .. .. .. .. . . . . . . . . . . . . .. . . . . . . .. .. .. .. .. .. .. .. .. .. .. .. .. .. .2-62.10 Disposal Of Associated Debris . .. .. .. .. . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-63. RECOMMENDATIONS AND CONCLUSIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. .. .. . . .. . . . . . . . . . . . . .3-14. REFERENCES . . . . . . . . . . . .. .. .. .... .............. . ... . .. .. .. .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . .. .. . 4-1AppendicesAppendix A - Archaeological ReportAppendix B - Laboratory ReportsAppendix C - Agenda and Sign-in Sheet for Public MeetingVOLUME IIData PackagesInvestigation of Geophysical Anomaly, Gambell, Alaska - FINAL J page iList of Figures1-I VICINITY MAP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-41-2 LOCATION MAP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-51-3 GAMBELL REMEDIAL INVESTIGATION SITES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-61-4 SAMPLE LOCATIONS AND GEOPHYSICAL BOUNDARIES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-71-5 SITE 5 GEOPHYSICAL RESULTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-82-1 SIVUQAQ, INC . HAZWOPER TRAINING - JULY 1997 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-72-2 SITE 5 INVESTIGATION OF GEOPHYSICAL ANOMALY # 1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-82-3 SITE 5 INVESTIGATION OF GEOPHYSICAL ANOMALY #2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-92-4 METAL DETECTION SCANNING . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-102-5 GROUNDWATER SAMPLING - NEW INFILTRATION GALLERY . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-112-6 MONITORING WELL DECOMMISSIONING . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-122-7 REMOVAL AND DISPOSAL OF THREE TRANSFORMERS FROM SITE 4/AREA 4D . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-13Investigation of Geophysical Anomaly , Gambell ,Alaska-FINALOpageiiList of AcronymsADEC Alaska Department of Environmental ConservationATV All-Terrain VehicleBTEX Benzene, Toluene, Ethylbenzene, and XylenesCDAP Chemical Data Acquisition PlanCFR Code of Federal RegulationsDERA Defense Environmental Restoration AccountDERP Defense Environmental Restoration ProgramDOD United States Department of DefenseDRO Diesel Range OrganicsE&E Ecology and Environment, Inc .FUDS Formerly Used Defense SitesGRO Gasoline Range OrganicsHAZWOPER Hazardous Waste Operations and Emergency ResponseMW Monitoring WellOSHA Occupational Safety and Health AdministrationPCB Polychlorinated BiphenylsPVC Poly-vinyl ChlorideQA/QC Quality Assurance/Quality ControlRI Remedial InvestigationRI/FS Remedial Investigation and Feasibility StudyRRO Residual Range OrganicsSOW Scope of WorkUSACE United States Army Corps of EngineersUSEPA United States Environmental Protection AgencyVOC Volatile Organic CompoundInvestigation of Geophysical Anomaly, Gambell, Alaska - FINALpage iiiINTRODUCTIONThe United States Army Engineer District, Alaska (Alaska District), requested that MontgomeryWatson investigate a geophysical anomaly reported to be buried transformers located near theonly active drinking water supply in the village of Gambell, St . Lawrence Island, Alaska . Thework was performed under contract No . DACA 85-93-D-0011, Delivery Order No . 16,Modification No . 3 . The investigation was performed in August, 1997 according . to theguidelines of the Final Work Plan Amendment for Investigation of Geophysical Anomaly(Montgomery Watson, 1997a) and the Defense Environmental Restoration Program of theUnited States Department of Defense .A previous delivery order provided for a geophysical survey of an area where transformers werereportedly buried near the water supply at Gambell . Results of the 1996 geophysical surveyconfirmed the presence and location of metallic debris, but the specific nature of the debris wasunknown . The objective of the current investigation was to ascertain whether the geophysicalanomaly was actually the reported transformers and whether any PCBs were associated with anytransformers present . This report describes the results of the investigation of the geophysicalanomaly .1 .1 PREVIOUS DOCUMENTSThe site description and background information contained in this report have been summarizedfrom previous documents about the Gambell site . Further site description and backgroundinformation can be found in the documents listed below .Draft Phase II Remedial Investigation, Gambell, St . Lawrence Island, Alaska . MontgomeryWatson . December 3, 1996 .Remedial Action Alternatives Technical Memorandum, Gambell, St . Lawrence Island,Alaska . Montgomery Watson . November 1995 .Remedial Investigation, Gambell, St . Lawrence Island, Alaska . Montgomery Watson .January 1995 .Chemical Data Acquisition Plan, Site Inventory Update, Gambell, St . Lawrence Island,Alaska . E&E . February 1993 .Site Inventory, Gambell, St . Lawrence Island, Alaska, E&E . December 1992 .The project description and objectives have been summarized from the Final Work PlanAmendment for Investigation of Geophysical Anomaly, Gambell, St . Lawrence Island, Alaska .Montgomery Watson, August, 1997 .Investigation of Geophysical Anomaly, Gambell, Alaska -FINALOpageI-I1 .2 SITE DESCRIPTIONGambell is located off the coast of western Alaska (Figure 1-1) on the northwest tip ofSt . Lawrence Island (Figure 1-2), in the western portion of the Bering Sea approximately 200 airmiles southwest of Nome, Alaska . Gambell is 39 air miles from the Siberian ChukotskPeninsula. The village of Gambell is built on a gravel spit which projects northward andwestward from the island . Gambell is at an elevation of approximately 30 feet above mean sealevel (MSL) .St . Lawrence Island is currently owned jointly by Sivuqaq, Inc ., in Gambell, Alaska, andSavoonga Native Corporation, in Savoonga, Alaska . Non-Native land on St . Lawrence Island islimited to state land used for airstrips and related facilities in Gambell (Montgomery Watson1995a) .The village of Gambell is inhabited primarily by native St . Lawrence Island Yupik people wholead a subsistence-based lifestyle . The Gambell area supports habitat for a variety of seabirds,waterfowl, and mammals that either breed in or visit the area . The area surrounding the top ofSevuokuk Mountain supports a large bird rookery . The birds and bird eggs serve as asubsistence food source for local inhabitants . The ocean surrounding the Gambell area is usedextensively for subsistence hunting of walrus, seals, sea birds, and polar bears .1 .3 BACKGROUND INFORMATIONA Phase I RI was performed in 1994 (Montgomery Watson 1995a) in which investigations wereperformed at eighteen sites, including the Former Tramway Site ; Site 5 (Figure 1-3) . Specificactivities performed at Site 5 during the Phase I RI included a geophysical survey, installing twoboreholes and two monitoring wells ; and collecting subsurface soil and groundwater samples forchemical analysis . Information on investigative activities and sampling results for the remainingGambell sites can be found in the Phase I and Phase II RI reports (Montgomery Watson, 1995a ;1996c) .Petroleum hydrocarbons were the contaminant of concern found in soils at MW 16 at depths to5 .0 feet . DRO was detected in soils at MW 16 at concentrations ranging from 1,160 mg/kg to1,800 mg/kg . Of primary concern at Site 5 is the human health risk posed by petroleumcontaminated soils in contact with groundwater used for the local water supply, and PCBs fromthe reported transformers . Volatile components of hydrocarbons were not detected in soil andgroundwater, and recent testing of the water supply indicates volatile contaminants are notpresent .Site 5 was retained for further investigation during the Phase II investigation , which involved theresampling of the two existing -monitoring wells for DRO and VOC analysis . In addition, since,the 1994 geophysical investigation showed no anomalous areas that would indicate the locationof the six, 8-foot long transformers reportedly buried at Site 5, the 1994 geophysical surveyboundary was extended to include a 200-foot by 200-foot area in order to locate the area wherelarge transformers were reportedly buried (Figure 1 -4) . Winfred ( Winnie ) James, a life longInvestigation of Geophysical Anomaly, Gambell, Alaska - FINALJpage1-2resident of Gambell, brought Montgomery Watson and Alaska District representatives to thereported transformer burial area during a community relations visit in March, 1996 . At the site,Winnie confirmed that the transformers would be found within the extended geophysical gridboundary later completed during the 1996 Phase II RI field work . A supplemental geophysicalinvestigation was performed in this area using the EM-31D terrain conductivity meter and theGSM-19 Overhauser Effect proton precession magnetometer/gradiometer during the 1996 fieldefforts .The local village drinking water supply is located near .Site 5 . The village water supply consistsof an infiltration gallery completed to a depth of 20 feet . The water supply facilities are housedwithin a building within a fenced area, as shown on Figure 1-4 .A large anomaly was found in the center of the 1996 geophysical survey grid in an area with novisible surficial conductive debris, as shown in Figure 2-5 . This anomaly was interpreted to be atrench orientated north-south filled with significant amounts of debris . Both the EM andmagnetometry surveys found strong evidence that this debris could possibly be the six secondarytransformers discussed in the Chemical Data Acquisition Plan (E&E, 1993) .The large anomaly located in the center of the grid has been designated "Anomaly #1 ." Asecond, smaller anomaly located near a large granite boulder in the southeast portion of the gridhas been designated "Anomaly #2 ." All other anomalies in the geophysical survey can becorrelated with metallic features visible at the surface, such as steel pipes or posts .Further geophysical information for Site 5 can be found in the 1994 Geophysical SurveyInvestigations Final Report (Golder, 1994) . Further site descriptions and backgroundinformation can be found in Section 1 of Montgomery Watson's Remedial Investigation Report(Montgomery Watson 1995a), the Remedial Action Alternatives Technical Memorandum(Montgomery Watson 1995b), and the Phase II Remedial Investigation Report (MontgomeryWatson, 1996c) .1 .4 PROJECT OBJECTIVEThe objective of this project was to excavate the two anomalous areas located in Site 5, identifythe buried metallic debris, remove, complete confirmation sampling and dispose of the debrisand any associated waste . General investigation procedures were established by the AlaskaDistrict, the City of Gambell, Sivuqaq, Inc ., Montgomery Watson, and two divisions of ADEC(the Contaminated Sites program and the Village Safe Water program) . The anomalyinvestigation activities performed during the 1997 field work are discussed in Section 2 .Investigation of Geophysical Anomaly, Gambell ,Alaska-FINALOpage1-3JOB No . 2198 .0420 TIME : k$$$SYTIMES$$$$$$ FILE : $$$$OGNSPEC$$$$$stssss$$*$$$$$$$$$ssssts!J° C'l'ark y///'°`'~,~///~ GAMBELL,i~ST . LAWRENCE ISLANDslsAp G/wd"'sO R TNONMaskr,rn~,GOiJ~i /Ro4t«.llkCt~y-~ ' 4 a.J /1i~kp C9R'Oe.eel poor~yI"~bJ, ~ 4 i~Yf"•ve 4 -kmraSlkn k C.p, ~/ ._(Ij1~~D :II` Chukon~'NomS.e,rtkrmr Cam°Mwaut CW~'. _aoP,Nemr""d-: twnukl,ka.drNendwt !Carbwr0KonFeMmnbncMngeUNEAj05PACIFIC OCEAN0600KILOMETERSMONTGOMERY WATSONAnchorage, AlaskaOFR TSOURCE : U .S. Geological SurveyFIGURE 1-1Reston, Virginia 22092, 1976.Lawrence,AlaskaALASKADISTRICT- CORPS OF ENGINEERSStN6265 - W16830 ,60x210 GAMBELL, ST . LAWRENCE ISLAND, ALASKASurveyed 1948, Compiled 1957Minor Revisions 1974Scale 1 :250,000 Contour Interval 100'VICINITY MAPGAMBELL.~: 4•,5t L& . a IslandQIAp S (.Io'°"'b~ .JOB No . 1189010 .161601FILE : $SSSOGNSPECS$SSSSSSSSSSSSS$SSSS$$$SS$SSS$TIME: SSSSSYTIMESSSSSSSGAMBELL,ST . LAWRENCE ISLANDBering SeaNorthwest Cap ~~~Chibukak PtGambel t . .: t' n ''Landing A reaTategnak Pt'-ATmar tn: nIJ~~' d"ot7£8n1Nkuk Mtnp , Tifldghak BayLakeltl ~1 ` .~~I Meruwlu PtOoynikP~n'~Tf20 5°rnln6aalir Pt / I,'t't?;i'C .~`Akeftapak,~ Akeftapak BayKaghoppalik Pl~C~~ Qe ••Ryp~\°~'° Op7a31'~ ~Nmgeehak° ~ C i eeacnKatalpha ,7BdI+-X64-\, t v Iw Agrist r t \, I . ~, . ' L-( A }v:n'- ! nUpapak pt,-/°y %s04~~ /_ ~° ~1 •~u ,Savukahul ''DShlokovik r~_vaE~Ki154 Pai. ?r rJ ° t`1a C'~ j 4Ktt.;Naskak Camp{j2Kineeghit4JkPak'VA6~s'. 1Pa9neo/t0S40/~n`'tea""';te O~'i ~j n ~:JTaphookt..1Icagnkusahk9GII`0fa~.~FvABy\k~t\=~aMONTGOMERY WATSONAnchorage, AlaskaSOURCE : U .S . Geological SurveyReston , Virginia 22092,1976St . Lawrence, AlaskaN6265 - W16830 , 60x210Surveyed 1948 , Compiled 1957Minor Revisions 1974Scale 1 : 250 .000 . Contour Interval 200'FIGURE 1-2IVORTHALASKA DISTRICT - CORPS OF ENGINEERSGAMBELL, ST . LAWRENCE ISLAND , ALASKALOCATION MAPGAMBELLNOTES :1 . Mapping taken from Chemical Data Acquisition Plan by Ecology &Environment (1993) . Map ing believ d to be sketched from aerial phot graphy taken in 19 5. Accuracy unknown .wESTaEACH-.2 . Plane Crash Site was not visited during 1994 RI .RUNWAYzpBERING SEA5NaW Plane Cnah approx. 7 miles so Oh ), Note2SUSPECTED ORDNANCEBURIAL SITE~Lp-°OLD GAMBELLG°C°°MJNICIPAL BuuurvGTROLTNUN LAKEPUMP HOUSE'~-- ~210~rAREA'~p0 -~-~,-11g•.'~1 0,;I1OYul~~jL ~l1~1~ARow~~G~~-__BURIA~,/3\-2TAANSFOA-0~I'EASVAREA IBAIR FORCELANDING AREAAREA 4D'~`J~~10rARMY TRAIL_____AREA ~4A__riIII-~ - .wTRAILFORMER AIA~ RAOAR SITEFORCE,\. SEVUOKL''__MNrrituFIGURE 1-3LEGEND :zTED OAD ANCESITEFORMER MILITARY HOUSING'OPERATI NS BURIAL SITEs` FA LIEN BURIIA UAREATIONEIr1AARr'/mAREA~ II ~5GUST,s~~IBURLAL~~WATER SUPPLY` `/~/TRANSFORMER~17iANI71NGNFIL RATION GALLERY ~_~ IE(NO' CI.ARENTLY USEDI~Op/iII.,NORTHBEACHARCHAEOIOGICAtsITEsul~~CAaCE BURIAL AREApap.A,NDFILL ND .2}~13-NORTH1.1C'1IIu\12° °°°° o o°°a IANDH,L NDQWATERTRANSMISSION~~° D°°c~ I i ' 7FORMER MAIN CAMP1994 SUM MER LAKE ''`` ~~1994M~/i~A UNNAMFnPONDO°VILLAGE OF WM9ELlti a o ~ ~o ~°~~~ °HIGH SCHOOLsoul ARan %'° OLO MLLAGE WELLI 0° 0 o-8NAYVAGH0.0LAKE°D ac oo D o ° q ° cm Do l000AACHAEOLOCIGA, SITEARMY LANDFILLO8~2G2D-J_'fSITE14(/8IpMONTGOMERY WATSONAnchorage, AlaskaBoundaryofSiteSCALE _ F~®o1200ALASKA DISTRICT - CORPS OF ENGINEERSGAMBELL, ST . LAWRENCE ISLAND, ALASKAGAMBELL REMEDIAL INVESTIGATIONSITESBoundary of 1994Geophysical Survey/New Well Housefor New InfiltrationGalleryiAnomal#1cvIl4 Al's/ Trail---------------Abandoned /MW 16 /I''~S lIE 5~'.-- Anomaly77 Digs #2BoulderBoundary of 1996 Geophysical SurveyNOTES :1 . Mapping by AEROMAP U . S ., Inc . from photography dated 7-12-1994for UNWIN SCHEBEN KORYNTA HUETTL .. This map conforms to National Map Standards as related to the projectphoto control for scales of 1"=100' or smaller .The vertical accuracy is approximately one half of the contour interval shownin any given area on the map . Contours in vegetated areas may be lessaccurate, contours in dense vegetation are likely to be less accurate .2 . Mapping taken from CRW Engineering Group, prepared by NorthPacific Aerial Surveys, Inc., date of photography 10-22-85 .SCALE IN FEET60120FIGURE 1-4W MONTGOMERY WATSONAnchorage, AlaskaU .S . ARMY ENGINEER DISTRICT, ALASKAGAMBELL, ST . LAWRENCE ISLAND, ALASKASITE 5 SAMPLE LOCATIONSAND GEOPHYSICAL BOUNDARIESJ.z050E100E150E1STEEL FREIGHT CONTAINER/PUMP STATION200EOON(ELEC TRic rY)- .y-HIo-i`¢.6"_VSTF( .- R05IIPIT-ti~ i.A G N :nDEEP_ANOMALY # 1_gZHUMMOCKY GRBU`; , 'Ts . - -.1,4-Difluorobenzene 79 .688 .1( 50-150 )( 50-150 )08/13/97 08/14/9708/13/97 08/14/97DRO/RRO CombinationDiesel Range OrganicsResidual Range organics GC0 .1031 .49 U0 .09951 .49mg/L08/13/97 08/15/97 WAA08/13/ 97 08/ 15/97 WAASurrogates5a Androstane c surr>d-Triacontane < Surr>70 .184 .8XXAK102/103mg/ Lmg/LSW846 8081AK102/103( 50-150 )( 50-150 )08/13/97 08/15/9708/13/97 08/15/97PCBs by GC ECDAroclor-10160 .00101 UAroclor-12210 .00101 U0 .00101 UicLor-12320 .001010 .001010 .00101mg/LSW846 8081SW846 808108/13/97 08/14/97 JLB08/13/97 08/ 14/97 JLB08/13/97 08 / 14/97 JLB4'ICT&E Environmental Services Inc .CT&E Ref.# 974607001Client NameMontgomery Watson Americas IncProject Name/# Gambell TransformersClient Sample ID 97GAMOIONVWMatrix Water (Surface, Eff., Ground)Ordered ByPWSIDParameterResultsPQLClient PO# ANC96CTE04Printed Date/Time 10 /13/97 12 :41Collected Date/ Time 08 /13/97 08 :30Received Date/Time 08 /13/97 17 :10Technical Director : Stephen C . EdeUnitsMethodSW846 8081SW846 8081SW846 8081SW846 8081Aroclor-1242Aroclor-1248Aroclor-12540 .00101 U0 .00101 U0 .00101 U0 .001010 .001010 .00101mg/Lmg/Lmg/LAroctor-12600 .00101 U0 .00101mg/LAllowableLimitsPrepDateAnalysisDateInit08/13/97 08/14/97 JLB08/13/97 08/14/97 JLB08/13/97 08/14/97 JLB08/13/97 08/14/97 JLB'arrogatesDecachlorobiphenyl Tetrachloro-m-xylene !68 .387 .6XXSW846 8081SW846 8081(59 - 122)(10-87)08 /13/97 08/14/9708/13/97 08/14/9711CT&E Environmental----- Services Inc .ICT&E Ref.#Client NameProject Name/#Client Sample IDMatrixOrdered ByPWSID~/I~II NI ~Il ~I974607002Montgomery Watson Americas IncGambell TransformersTrip BlankWater ( Surface , Eff ., Ground)ParameterClient PO#ANC96CTE04Printed Date /Time10/13/97 12 :41Collected Date/ Time 08/13/97 08 :30Received Date/Time08 /13/97 17 :10Technical Director : Stephen C . EdeReleased ByResultsPCLAllowableLimitsPrepDateAnalysisUnitsMethod0 .04000 .00100 .0010mg/Lmg/Lmg/L08/13/97 08/14/97 GSM0 .00100 .00100 .0010mg/Lmg/Lmg/LAK101/8020AK101 /8020AK101/8020AK101 /8020AK101/8020AK101/802008/13/97 08/14/97 GSM08 /13/97 08/14/97 GSM08/13/97 08/14/97 GSMDateInitGRO/602 Combo-'asoline Range Organicsizene,olueneEthytbenzeneP & M -Xyleneo-Xylene0 .0400 U0 .0010 U0 .0010 U0 .0010 U0 .0010 U0 .0010 U08/13/97 08/14/97 GSM08/13/97 08/14/97 GSMSurrogates4-Bromofluorobenzene 1,4-Difluorobenzene 077 .988 .1AK101/8020AK101/8020(50-150)( 50-150 )08/13/97 08/14/9708/13/97 08/14/97MONTGOMERY WATSONTo:FileFrom:Date:Bonnie McLeanReference :Subject :Gambell Village Water SupplySamplingAugust 22, 19971189010 .161605On July 24 , 1997, Bonnie McLean collected a water sample (ID : 97GAM 001 N V) from theVillage of Gambell ' s New Water infiltration gallery. Pump #2 was allowed to run 10 minutes bythe operator , Iver Campbell . A sample was collected at 8 a .m ., and submitted for analysis forDiesel Range Organics ( DRO) (Method AK102) and Volatile Organic Compounds (VOC)(Method 8100 M), packed in a cooler containing frozen gel ice, and sealed with a custody seal .Weather prevented transport from St . Lawrence Island until July 26 , 1997 . During the wait, thesample was kept chilled (4°C+ 2°C ) and was locked in the samplers ' quarters . Upon arrival inAnchorage the sample was maintained under the control of the sampler and chilled until it wasrelinquished at CT & E Environmental Services on July 28, 1997 at 8 : 35 a .m. The laboratorywas made aware of the shortened extraction time remaining verbally , and noted on the Chain-ofCustody .cc : Victory HarrisMerle AppasingokSuzanne Beauchamp/dw/1189010 .161605CT&E Environmental Services Inc .L_ IZtElorm,Laboratory DivisionCHAIN OF CUSTODY_~PO#:Reports to:Invoice to:A~--t~-Special Instructions :IT~•QUOTE #0 0 rLaboratory:Page I of ICT&E Environmental Services Inc .200 W Potter Dr.Anchorage, AK 99518-1605Phone (907) 562 -2343 Fax : (907) 561-5301(~~•r•JC'c ccjr VJ rf~t-tt o- % .GC- (/ /c .Phone :Fax: .f-C(B'C S `fContact person for questions concerning these samples :97 .4076 _j01N_ c (._ a r.Phone :f I `t Fax: Z 4< SY5 s 7'N ofContainerLab ISam le Recei' ~. . . . . B :cNumber of ContainersCOC Seals/Intact Y/N/NATemperatureTurnaround RequiredData Deliverables RequiredLevel lLevel li vel illis. ..:NwTimeN.. .:Rowvad By:ivied B3 :D"':DowReceived at Laboratory By- =1 kT"'c1rV \ e o V\ow97 .4607Montgomery Watson USCOE4100 Spenard Road GAMBELLAnchorage AK 99517(907)248-8883Fax(907) 248- 8884•WASTELaboratoryry_CaSSi+a0MCMLEI00amp ers :SignatureDate-~~w/`(t f ~l_ w lTimeSample IDTotalContainers4ozAmber20 mlMeOH4ozAmberNone4ozAmber20 mlMcOH2 . 1-liter 2 . 1-liter 7, 40-m1AmberAmbervialsNoneNoneHCL002 , 1-literAmberNone2, I-literPE, 250ml PENone2 , 40 mlNoneSurgicalswabHexanemRelinquished by :R 'ved,' 12aboVby :_DateTimeDateTimeHand DeliveredY$ 310Shipped Via Airbill Number ,s y /Cooler Temperature aC Laboratory NotifiedUpon Arrival FaxedDateTimeAppendix CAgenda and Sign-in Sheetfar Public MeetingMONTGOMERY WATSONAgendaPublic Meeting in GambellSuspected Buried Transformer InvestigationJuly 23, 1997 7 :00 p.m.Available for Questions:Alaska District, Corps of Engineers : Suzanne Beauchamp, Engineering ManagerSivuqaq, Inc. : Merle Apassingok, PresidentAk. Dept. of Environmental Conservation : Katarina Rutkowski, Envir . SpecialistMontgomery Watson : Victor Harris, Project MangerMontgomery Watson : Bonnie McLean, Field SupervisorTopics to Be Discussed:I, IntroductionII. Background of the InvestigationIII. Project Activities and ScheduleIV . Water ConservationV . Door PrizesVI. Open Discussion/Questions0MONTGOMERY WATSONBYyS_OATE7l Z S7 CLIENTCHKD. BYDESCRIPTIONSfif7d.L~IOleAs AV .3 Sic'99/93L4 D3z3 t.a'2ce Lt~ Qr/D-d;tut~o. A:Aqqq41CM, 4,11q,C~L~sl a L.Q9.w I (,fWl4q. etw.&Ar C,=~p4tAj a:=O ttty%V°•SAt t~~.S'1~ .52. (11/~Ot, - .~ 063.5`(. ^a a'~ ~~e -~-C0EN 1S (10/78)SHEETw~OF130 MAR 1998CEPOA- EN-EE -II (200-1c)MEMORANDUM FOR CEPOA-EN-G (Thomas)CEPOA-EN-EE-TE (Gagnon)CEPOA-EN-CW-ER (McConnell)SUBJECT : Contract No . DACA85-93-D-0011, Delivery Order No . 16,Modification No . 3, Final Report, Investigation of GeophysicalAnomaly, Gambell, St . Lawrence Island, Alaska, December 19971 . Enclosed for your information is a copy of the subject reportfor your records, which describes activities performed duringAugust 1997 to identify and remove objects at a suspectedtransformer burial site . Review comments and responses are alsoincluded .2 . Please note that Volume II, Data packages, was assembled aspart of the response to comments . A copy of Volume II isincluded in the CEPOA-EN-G package only .3 . If you have any questions concerning the enclosed report orany other Gambell RI/ FS issues , please contact me at (907) 7535606 .2!~) ~J EL~'EnclRichardJacksonEngineering ManagerI TVIECOMNVPROJECT :Investigation of Geophysical AnomalyNT S DOCUMENT : ,Final Report (Montgomery Watson , December 1997)LOCATION :?J .S . ARMY CORPSOF ENGINEERSCENPA-EN-CW-ERGambell, St. Lawrence Island , AlaskaDATE : December 12, 1997REVIEWER : Guy R. McConnellPHONE :Action taken on comment by :Location (pg#, para, etc .)COMMENTSI.page2pageItel SNoBonnie McLeanREVIEW CONFERENCEA - comment acceptedW - comment withdrawn(if neither, explain)DESIGN OFFICEC - correction made(If not, explain)The report should state the current status of the artifact such as whetherit was returned to the existing Native village or kept by the archaeologist .A:Text and Appendix A(page 6 ), archaeologist(Pg 2-3) reportcorrected .The report also should state whether the existing Native Village wasconsulted regarding the reburial of the human remains . This consultationA : Text added (page 2 -3) .Text added ( page 2-3) .A : CorrectedCorrectedshould have been part of the project and is required under Federallegislation particularly in this case, the Native American GravesProtection and Repatriation Act .PageTypo on Page 6, paragraph 2, should read planing adze bit, not planningadze bit .IiSHT . 1 Of 2Backcheckby :REV][E PROJECT : Investigation of Geophysical Anomalyk- F ANTS DOCUMENT : Final Report (Montgomery Watson , December 1997)LOCATION : Gambell, St. Lawrence Island , AlaskaJ .S . "-R-MY CORPSOF 1,NG-VEERSCENPA-1,N-CW-ERDATE : December 13, 1997REVIEWER : KissingerPHONE :Action taken on comment by :IterrNo .Location (pg#, para, etc.)COMMENTSIp eBatch QC data is missing . Data for surrogate recovery is included butdata for batch LCS, matrix spikes and method blanks are missing .Bonnie McLeanREVIEW CONFERENCEA - comment acceptedW - comment withdrawn(if neither, explain)DESIGN OFFICEC - correction made(If not, explain)A : Data added as Volume II ,text added to report 2.7.3C -Data added asVolume II, text added toreport 2 .7 .3MS/MSD was notrequired at time ofsampling .iSHT. 1 Of 2Backcheckby :REVIEWPROJECT:Investigation of Geophysical AnomalyC (]1_\ 1 NTS DOCUMENT : Final Report ( Montgomery Watson , December 1997)LOCATION :U ., . A ZMV CORPS0 ' El` GINEL RSCl .NP_ i-EN-C W-ERIt( inI >.(.Location (pg4r, para, etc .)Tpage 2-4°DATE : December 12, 1997REVIEWER : Bret L . WaltersPHONE:Gambell, St. Lawrence Island , AlaskaAction taken on comment byCOMMENTSSection 2 .7 .2 : The fourth sentence should end as follows . "in the pre-andpost-excavation samples, respectively ." .Bonnie McLeanREVIEW CONFERENCEA - comment acceptedW - comment withdrawn(if neither, explain)DESIGN OFFICEC - correction made(If not , explain)A:C -SHT, 1 Of 2Backcheckby :CEPOA-EN-CW-ER.DEC 4 1991MEMORANDOM FOR CEPOA-EN-EE-II (Jackson)SUBJECT : Comments regarding report for Contract No . DACA85-93-D-0011,Delivery Order No . 16, Modification No . 3, Draft Report, Investigationof Geophysical Anomaly, Gambell, St . Lawrence Island, Alaska, October1997 .1 . The report should state the current status of the artifact such as,whether it was returned to the existing Native village or kept by thearchaeologist .2 . The report also should state whether the existing Native Village wasconsulted regarding the reburial of the human remains . Thisconsultation should have been part of the project and is required underFederal legislation particularly in this case, the Native AmericanGraves Protection and Repatriation Act .3 . Typo on Page 6, paragraph 2, should read planing adze bit, notplanning adze bit .Guy R . McConnellBiologistHTRW-CX COMMENT TRANSMITTALComments Transmitted toCommander,Alaska DistrictCEPOA, Richard JacksonAttentionSubmittal #000997 - 65182ActionProjectInformationComments are transmitted with this record .LocationSiteProjectSt Lawrence IslandGambellSite WideDoc TitleDraft Report, Investigation of Geophysical An omaly, Gambell, St Lawrence Island, AKPhaseDesigned byDraftMontgomery Watson , AnchorageDISCIPLINE ACTION'ChemistryRCAGeotechnical NCHealth &Safety12/05/97SIGNIFICANT OR UNRESOLVED TECHNICAL COMMENTSChem : Much of the analytical QC data is missing from the lab report .NCRisk Assessment NCStudies / Liaison ---REQUESTED ACTIONTo further our understanding of the iss ues that affect this project and yourrlic_trirt'S execution, please provide this office a copy of annotated responses tocomments made by your office , other agencies and interested parties .HTRW-CX Point of Con `act ,[~ tTelephone :Hel 1 Novotny(402) 697-2626Transmittal of comments approved by :Ken L : Gr gg, P .E .Chief, Environmental Studiesand Liaison Branch'NC = Reviewed ; No Comments NT = No tech involvment CT = Conferred/Deferred to District CounterpartRCA = Reviewed , Comments Attached SCA = Reviewed w/Significant Comments attached[X] CEPOA -EN-EE-AI Richard Jackson[]POD[) CENWO-HXS Heidi Novotny[ ] CENWO-HX-S (Files)65182 : Investig of magnetic anomaly at St . Lawrence Island , AK - Draft ReporFile : 65182RDK .DBFeTemp ID2344055-462Page : 1Last NameOffice SymbolKISSINGERCENWO-HX-CDisciplineCHEMPage/Sheet Room DtlPost ITAppendix BBatch QC data is missing . Data for surrogate recovery is included but data for batch LCS, matrix spikes and method blanksare missing .This information should be included to support data quality .Printed 11 /25/97 2 :49 :31 PM-FINALInvestigation of Geophysical AnomalyGambell, St . Lawrence Island, AlaskaContract No . Delivery Order No .DACA85-93-D-001 1 0016Modification No . P0003VOLUME IIDATA PACKAGESDecember 1997Prepared for :Department of the ArmyUnited States Army Engineer District, AlaskaCorps of EngineersP.O. Box 898Anchorage, Alaska 99506-0898Prepared by :Montgomery Watson4100 Spenard RoadAnchorage, Alaska 99517VOL2OF2ME Environmental Services Inc .Alaska DivisionLaboratory Data ReportContents :Section 1 : Case Narrative Information (COC, etc .)Section 2 : CTE Final ReportsSection 3 .1, 4.1, 5 .1 . . . :Section 3 .2, 4 .2, 5 .2 . . . :Section 3 .3, 4 .3, 5 .3 . . . :Quality Control Summary FormsInitial CalibrationsRaw Analytical Data, if requiredSections 3 and above are arranged consecutively in the following fashion : Volatiles, SemiVolatiles,Metals , Inorganics, Miscellaneous .Note: All quality assurance/quality control criteria is in compliance with the Alaska Departmentof Environmental Conservation (ADEC) and/or CTE's Assurance Program Plan .Prepared by (Signature)(Printed Name)(Date)Reviewed by (Signature)(Printed Name)(Date)%- 1N_ 1 1~its (11 .I_- a9 - 9 -1Case NarrativeCustomer: JMMENGN Montgomery Watson Americas IncProject:974607 Gambell TransformersThere were no analytical anomalies associated with your data .Page 1Report SummaryLabrepoampsa sampirxnmco aWSCS AK101WSWSCS AK102ECS SW8081WSCS AK101WSWSSDI AKIOIBSI AKIOIWSWSxmco a og a ex a eA na a ea o cKunSW5030A 08/13/97SW3510 08/1319708/13/9708/13/9708/14/9708/15/972640VXX3120XXX1SW3510 08/13/97SW5030A 08/13/9708/13/9708/14/973110XXX1108/13/9708/14/972640VXX1SW5030A / /08/13/9708/14/9708/13/9708/14/972640VXX2640VXX1CC1 AK101SW5030A / /NONE//WSCC2 AK101CC3 AKIOINONE//NONE / /08/13/9708/13/9708/13/9708/13/97WSWSCC4 AKIOILB1 AKIOINONE//SW5030A / /08/14/9708/14/9708/14/9708/14/97WSWSBD1 SW8081BS1 SW8081SW3510 / /08/13/97WSBS2 SW8081SW3510//SW3510 / /WSWSWSBS3 SW8081CC1 SW8081CC2 SW808108/13/ 9708/13/ 97WSCC3 SW8081NONENONE/ l//WSWSCC4 SW8081CC5 SW8081NONENONE/ /WSLB1 SW8081WSWSBD1 AK102EBSI AK102E113804113805WSCC1 AK102E113806WSWSWSCC2 AK102ECC3 AK102ECC4 AK102EWSWSCC5 AK102ECC6 AK102EWSCC7 AK102ENONE/ /NONE / /WSLBI AK102ESW3510 / /97460797GAMO10NVW97460797GAMOIONVW97460700197460700197460797460797GAM010NVWTrip Blank974607001974607002113554113553113566113567114787114788113552113016113015113017113018113621113622113623113624113620113014113512113511113809113834113835113802113510SW3510 / /NONE//08/13/9708/14/9708/14/9708 /14/972640VXX112640VXX2640VXX112640VXX2640VXX113110XXX1311OXXX3110XXX113110XXX3110XXX1108/13/9708/14/9708/14/9708/14/9708/14/9708/14/9708/ 14/9708/14/ 9708/15/9708/14/973110XXX3110XXX111SW3510/ // /08/14/ 9708/15/9708/14/973110XXX3110XXX08/13/9708/14/973110XXX11SW3510/ /08/13/97SW3510 / /NONEI I08/13 /9708 / 15/9708 / 15/973120XXX1312OXXX312OXXX1108/14/9708/14/973120XXX11NONE/ /NONENONE/ // /NONE/ /08 / 15/9708/14/9708/14/9708/15/97312OXXX312OXXX08/14/9708/15 /9708/14 /9708/14 /9708/14/97312OXXX3120XXX08/15/97312OXXX08/15/9708/13/9708/15/9708115 /973120XXX11111u9704607Cc( -WASTEMontgomery Watson USCOE LaboratoryGAMBELL4100 Spenard RoadAnchorage AK 99517(907)248 -8883 Faxq(907) 248- 8884•CLM nyco, ,Dr^5~3mplers :Signature'Dale(vkr1Ol\Sample IDTotalContainers1 r 1 6\AAI03Q¢4ozAmber4ozAmberozAmbervby : ^20 mlMcOHos~<ac<a2, 1-literAmber2, 1-literPE, 250ml PE0None20 mlMcOH3us2, I-liter 2 , I-liter 1, 40 - mlAmberAmbervialsNoneNoneHCLa,Noneit3n~1None00003vt2 , 40 mlNone0cc3.titaui°d ..SurgicalswabHexaneZn (i r CRc, ved for Laboras-~TimeRelinquished by :oDateHand DeliveredTimeDate %Time1311 l UYW,Shipped Via Airbill Numbercq2-)!j yCooler Temperature oC Laboratory NotifiedUpon Arrival Faxed/DateTimeAMIArmy Corp of Engineers Project :%I-YES 0 NO Chem Lab RefComputer W/O# :Lab Due Date:/97 .4607(new) Account #Extraction Date:Holding Time :Client Name: G A,tits~ trOrdered By :Date Due :(iVia: oSample Received : gTime:Purchase Order#:Date Collected Time :Requisition#:Address :Paid (Ck#) (Cash)Amount S:Send Additional Reports to:Phone #:Fax :Phone #pecia!l tnstrncaionc('0Fax #O190C6IEP ToxH20-Meta>s Mien: O/0Sample RemarksChain Of Custody.Custody Seals:Recd By:Logged By:Entered By:Proofed By :10NYITemps. of SampleseSampleConditionsS le C 13IL97 .4607FPoorLI ECT&E Environmental Services Inc .Laboratory Division200 W . Potter DriveAnchorag .. AK 99518-1605SAMPLE RECEIPT CHECK LIST Fo (9907) 561.51Is sample temperature between 2.5 - 6 .0 °C?What is the sample temperatureAre samples within holding times?Were correct container and sample size submitted?Were preservatives checked?The required preservatives found?Do results go to ADECIs the P .W.S .LD.# given with samplesIs this a Corp of Engineers project?NONote #NONONONONONONOAdditional Information Required on all Corp of Engineers ProjecDate Received:' tSDate Opened:11 :6Date Logged in:$CTdtE# of CoolersBy Who (print)mil) CgSkeBy Who (print)54 `+ I )Was there a shipping slip (airbill # 4 2 2 -'seals?MSDcoolersealedwithcustodyWas theWere these seals intact upon arrival?Was there a chain of custody (COC) with cooler 0SWere the COC's filled out properly?Did the COC indicate samples from a COE project? EWere all samples listed on COC accounted forWere samples packed to prevent breakage? SWere bottles unbroken apd clearly labeled?Were bottles sealed in separate plastic bags?Was there headspace in bottles for volatiles?NONote #NONONONONONONONONONONOTES:Was client notified of problems? YES NO Dateltime :Who was notified? By whom? :How was this person notified?Was a copy of this form faxed for confirmation?Fax # sent to:Member d the $0a Group ISoe " GendraM da Surwill.nc./ENVIRONMENTAL FACILITIES IN ALASKA. CAUFORNIA . FLORIDA . ILLINOIS, MARYLAND, MICHIGAN . MISSOURI. NEW JERSEY . OHIO. WEST VIRGINIFCode ListCodeName! Out of control limits1 C First Column Result - The Value Obtained from the First Column2C Second Column Result - The Value Obtained from the Second Column< Less ThanEqual To> Greater ThanAELF American Environmental Laboratories, Pensacola, FLAENP American Environmental Network, Portland, ORALTC Alta Analytical Lab Incorporated, El Dorado Hills, CAAPPL Agriculture & Priority Pollutants Laboratories, Fresno, CAARDL Applied Research and Development Lab, Inc ., (ARDL) Mt. Vernon, ILARI Analytical Resources, Inc., Seattle, WAATCA Analytica, Anchorage, AKATCC Analytica, COATIA Analytical Technologies, Inc ., Anchorage, AKATIR Analytical Technologies, Inc ., Renton, WAATIS Analytical Technologies, Inc ., San Diego, CAATOX Air Toxics LTD, Folsom, CABCLB BC Laboratories, Bakersfield, CABD Blank Spike DuplicateBMLA Boreochem Mobile Lab & Analytical ServicesBRS Brelje & Race, Santa Rosa, CABS Blank SpikeCASA Columbia Analytical Services, Inc ., Anchorage, AKCASB Columbia Analytical Services, Inc ., Bothell, WACASK Columbia Analytical Services, Inc ., Kelso, WACC Continuing Calibration VerificationCCAC Coast-to-Coast Analytical Services, Inc ., Camarillo, CACCSJ Coast-to-Coast Analytical Services, Inc ., San Jose, CACDM CDM Federal Programs CorporationCHEM Chemic Laboratory, San Diego, CACKY CKY Inc ., Torrance, CACLPA Contract Laboratory Program Accuracy Limits for Spiked SamplesCLPCC CLP Continuing Calibration Acceptance CriteriaCLPIC CLP Initial Calibration Acceptance CriteriaCLPLR Contract Laboratory Program Precision for Lab ReplicatesCLPP Contract Laboratory Program Precision Limits for Spiked SamplesCLTP Clayton Environmental Consultants, Inc ., Pleasanton, CACS Client SampleCTB Curtis & Tompkins, Berkeley, CACTE CT&E Environmental Services, Inc ., Anchorage, AKDDL Method Defined Detection LimitDMP D & M Laboratories, Petaluma, CADOWL Dowl Engineering Alaska Test Labs, Anchorage, AKEBAEBAECEN Ecology & Environment, Inc .ECI EcoChem, Inc .EQL Estimated Quantitation LimitETCS ETC, Santa Rosa, CAFORA Forensic AnalyticalIC Initial Calibration VerificationIDL Instrument Detection LimitIN Internal StandardCodeNameKD Known (External Reference Material ) DuplicateLAB1 Laboratory ILAB2 Laboratory 2LAL Lockheed Analytical Laboratory, Las Vegas, NVLAS LAS Laboratories, Inc .LB Lab BlankLCC Laboratory Continuing Calibration AccuracyLDC Laboratory Data ConsultantsLIC Laboratory Initial Calibration AccuracyLLD Lowest Level of DetectionLLR Laboratory Established Precision for Lab ReplicatesLR Lab ReplicateLSA Laboratory Sample Accuracy for Spiked . SamplesLSP Laboratory Sample Precision for Spiked SamplesLTL Laucks Testing Lab, Inc.MASA MultiChem Analytical Services, Anchorage, AKMASR MultiChem Analytical Services, Renton, WAMDL Method Detection LimitMEA Method Established Accuracy for Spiked SamplesMECC Method Established Continuing Calibration Acceptance CriteriaMEIC Method Established Initial Calibration Acceptance CriteriaMELR Method Established Precision for Laboratory ReplicatesMEP Method Established Precision for Spiked SamplesMLR Matrix Laboratory Replicate PrecisionMS GC/MS Result - Value Confirmed Using GC/MSMS Lab Matrix SpikeMSA Matrix Spike Accuracy for Spiked SamplesMSP Matrix Spike Precision for Spiked SamplesNA Not ApplicableNA Not Available - Result Not AvailableNC Non-Client SampleNCAB North Creek Analytical, Bothell, WANCAP North Creek Analytical, Beaverton, ORND Not DetectedNETB NET Burbank, Burbank, CANETC NET Cambridge, Bedford, MANETO NET Portland, Portland, ORNETS NET Pacific, Inc ., Santa Rosa, CANR Not Reported - Data Not ReportedNTL Northern Testing Laboratories, Anchorage, AKNU Not Usable - Data Not UsableOEIR OnSite Environmental, Inc ., Redmond, WAPAC Pacific Analytical, Carlsbad, CAPARA Paragon Analytics, Inc., COPHLE Philip EnvironmentalPIC Pace Analytical Services, Inc ., Camarillo, CAPIHB Pace Analytical Services, Inc ., Huntington Beach, CAPIL Pace Analytical Services, Inc ., Lenexa, KSPIM Pace Analytical Services, Inc ., Minneapolis, MNPIN Pace Analytical Services, Inc ., Novato, CAPINY Pace Analytical Services, Inc ., New York, NYPIP Pace Analytical Services, Inc ., Pittsburgh, PAPITB Pace Analytical Services, Inc., Tampa Bay, FLPIWF Pace Analytical Services, Inc., Wappingers Falls, NYPQL Practical Quantitation LimitL.oaeNamePR Primary Result - The Primary Result for a ParameterPRL Parameter Range LimitQALA Quality Analytical Laboratores , Inc ., Montgomery, ALQALC Quality Analytical Laboratories , Inc ., Redding, CAQES Quanterra Environmental Services , Santa Ana, CAQESA Quanterra Environmental Services , Arvada, COQuanterra Environmental Services , North Canton, OHQESCQESFQuanterra Environmental Services, Tampa, FLQESGQuanterra Environmental Services , Garden Grove,QESI Quanterra Environmental Services , City of Industry, CAQESJQuanterra - Research Triangle Park Lab ., Raleigh, NCQESKQuanterra Environmental Services , Knoxville, TNQESL Quanterra Environmental Services , St. Louis, MOQESN Quanterra Environmental Services , Anchorage, AKQESP Quanterra Environmental Services , Pittsburg, PAQESRQuanterra Environmental Services , Richland, WAQESSQuanterra Environmental Services, Sacramento, CAQESTQuanterra Environmental Services , Austin, TXQESZQuanterra Environmental Services , Anchorage, AKRMKnown ( External Reference Material)RS Reagent SolventSAS Sound Analytical Services , Inc ., Tacoma, WASBSA Both Reagent and Matrix Sample Accuracy for SurrogatesSBSP Both Reagent and Matrix Sample Precision for SurrogatesSC3SS-Cubed , A Division of Maxwell Laboratories, Inc ., San Diego, CASCLAContract Laboratory Program Limits for Surrogate AccuracySUPContract Laboratory Program Limits for Surrogate PrecisionSD Lab Matrix Spike DuplicateSLSA Laboratory Sample Limits for Accuracy for SurrogatesSLSP Laboratory Sample Limits for Precision for SurrogatesSMEAMethod Established Limits for Accuracy for SurrogatesSMEP Method Established Limits for Precision for SurrogatesSMSASample Matrix Limits for Accuracy for SurrogatesSMSP Sample Matrix Limits for Precision for SurrogatesSPEC Spectra Laboratory , Inc., Tacoma, WASRAD Standard Reference Accuracy Defined by Agency/ManufacturerSRMA Standard Reference Material Accuracy Limits Determined by LabSRMP Standard Reference Material Precision Limits Determined by LabSRPD Standard Reference Precision Defined by Agency / ManufacturerSU SurrogateSWAA Shannon & Wilson , Inc ., Anchorage, AKSWLB Southwest LaboratorySWRI Southwest Resarch Institute , San Antonio, TXTI Tentatively Identified CompoundTRID Triangle Laboratories , Inc ., Durham, NCCT&E Environmental Services Inc .IL 3) Laboratory DivisionLaboratory Analysis ReportAugust 15, 1997Chris BrownMontgomery Watson Americas Inc4100 Spenard RdAnchorage , AK 99517-2901Client NameProject IDPrintedMontgomery Watson Americas IncGambell Transformers [974607]August 15, 1997Enclosed are the analytical results associated with the above project .As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Programis maintained by CT&E . A copy of our Quality Control Manual that outlines this program is availableat your request.Except as specifically noted, all statements and data in this report are in conformance to theprovisions set forth in our Quality Assurance Program Plan .If you have any questions regarding this report or if we can be of any other assistance , please callyour CT&E Project Manager at (907) 562-2343 .The following descriptors may be found on your report which will serve to further qualify the data .U - Indicates the compound was analyzed for but not detected .J - Indicates an estimated value that falls below PQL, but is greater than the MDL .B - Indicates the analyte is found in the blank associated with the sample .* - The analyte has exceeded allowable limits .GT - Greater ThanD - Secondary Dilution;LT - Less Than:! - Surrogate out of range200 W. Potter Drive, Anchorage , AK 99518- 1605 - Tel: (907) 562-2343 Fax : (907 ) 561-53013180 Pager Road , Fairbanks, AK 99709 - 5471 - Tel : (907) 474-8656 Fax : (907 ) 474-9685ENVIRONMENTAL FACILITIES IN ALASKA . CALIFORNIA , FLORIDA, ILLINOIS , MARYLAND, MICHIGAN , MISSOURI, NEW JERSEY, OHIO, WEST VIRGINIA.ALCT& E Environmental Services Inc .I H yI ~• IIH I H/~I yiI ~H/eI yCT&E Ref.#Client NameProject Name/#Client Sample IDMatrixOr dered ByPWSID974607001Montgomery Watson Americas IncGambell Transformers97GAMO1ONVWWater ( Surface, Eff., Ground)Client PO#ANC96CTE04Printed Date/Time08/15/97 16 :18Collected Date/Time 08/13/97 08 :30Received Date/Time 08/13 /97 17 :10Technical Director : Stephen C . EdeReleased By o~-^Sample Remarks :ResultsParameterPCLUnitsMethodAllowableLimitsPrep AnalysisDate Date InitGRO/602 ComboGasoline Range OrganicsBenzeneToluene7thylbenzene.' & M -Xyleneo-Xylene-0 .0400 U0 .0010 U0 .0010 U0 .0010 U0 .0010 U0 .0010 U0 .0400 mg/L0 .0010 mg/L0 .0010 mg/L0 .0010 mg/L0 .0010 mg/L0 .0010 mg/LAK101 / 8020AK101 / 8020AK101 / 8020AK101/802008/13/97 08/14/97 GSM08/13/ 97 08/14/97 GSM08/13/97 08/14/97 GSM08/13/97 08/14/97 GSM08/13/ 97 08/ 14/97 GSM08/13/ 97 08 / 14/97-GSMAK101/8020AK101 / 8020Surrogates4-Bromofluorobenzene 1,4-Difluorobenzene 79 .688 .1XXAK101 / 8020AK101 / 8020(50-150 )( 50-150 )08/13/9 7 08/14/9708/13/97 08/14/97DRO/RRO Combi nat i onDiesel Range OrganicsResidual Range Organics GC0 .1031 .49 U0 .0995 mg/L1 .49 mg/LAK102/103AK102/10308/ 13/97 08 / 15/97 WAA08/ 13/97 08 / 15/97 WAASurro g ates5a Androstane d-Triacontane 70 .184 .8XXAK102 / 103AK102/103(50 - 150)( 50-150 )08 / 13/97 08/15/9708/13 /97 08/15/97PCB's by GC ECOAroctor- 1016Aroctor° 1221ArocLor-1232Aroctor-1242Aroctor-12480 .00101 U0 .00101 U0 .00101 U0 .00101 U0 .00101 U0 .00101 mg / L0 .00101 mg / L0 .00101 mg/L0 .00101 mg/L0 .00101 mg/LSW846 8081SW846 8081SW846 8081SW846 808108/13/97 08 /14/97 JL808/13/97 08/14/97 JLB08/13/97 08/14 /97 JLS08/13 /97 08/14/97 JLBSW846 808108/13/97 08/14/97 JLBALCT&E Ref.#Client NameProject Name/#Client Sample MMatrixOrdered ByPWSIDCT&E Environmental Services Inc .Client PO#ANC96CTE04Printed Date/Time08/15/97 16 :18Collected Date/Time 08/13/97 08 :30Received Date/ Time 08/13/97 17 :10Technical Director: Stephen C . Ede974607001Montgomery Watson Americas IncGambell Transformers97GAMOIONVWWater (Surface, Ef ., Ground)Allowable Prep AnalysisParameterResultsPQLUnitsMethodmg/Lmg/LSW846 8081SW846 8081XSW846 8081XSW846 8081Limits Date Date!nitSurrogatesAroctor-1254Aroctor-12600 .00101 U0 .00101 U0 .001010 .0010108/13/97 08/ 14/97 JLB08/13/97 08/14/97 JLBSurrogatesDecachtorobiphenyl < Surr>Tetrachloro - m-xylene !68 .387 .6( 59-122 )( 10-87 )08/13/97 08/14/9708/13 / 97 08/14/97LT'..CT&E Environmental Services Inc.ANC96CTE04Client PO#08/15/97 16 :18Printed Date/TimeCollected Date/Time 08/13/97 08 :30Received Date/Time 08/13/97 17 :10Technical Director : Stephen C . EdeCT&E Ref .# 974607002Client Name Montgomery Watson Americas IncGambell TransformersProject Name/#Client Sample ID Trip BlankMatrix Water (Surface , Eff., Ground)Ordered ByPWSIDReleased BySample Remarks:Allowable PrepParameterPQLResultsUnitsMethodmg/Lmg/Lmg/Lmg/Lmg/Lmg/LAK101/8020AK101/8020AK101 /8020AK101/8020AK101/8020AK101/8020XXAK101 / 8020AK101 / 8020-Limits DateAnalysis .Date/nitGRO/602 ComboGasoline Range OrganicsBenzeneToluene7thylbenzene- & M -Xyleneo-Xylene0 .0400 U0.0010 U0 .0010 U0 .0010 U0 .0010 U0 .0010 U0 .04000 .00100 .00100 .00100 .00100 .001008/13 / 97 08/14/97 GSM08/13 /97 08 / 14/97 GSM08/13 /97 08/14/97 GSM08/13 /97 08/14/97 GSM08/13 /97 08/14/97 GSM08/13 /97 08/14/97 GSMSurrogates4-Bromoftuorobenzene 1,4-Difluorobenzene < Surr>77 .988 .1( 50-150 )( 50-150 )08/13 /97 08/14/9708/13/97 08/14/97Volatiles Sample QC Summary PageCT&E. Environmental Services Inc .QA/QC Data DeliverablesAnalysis Lot Number:VDA06060813Prep Lot Number : -7'Workorder Number:Analysis :Aromatic Volatile Organics /Gasoline Range OrganicsMethod : BTEX by EPA 8020/602/AK10I (8015M)Matrix :Solid/LiquidAnalysis:Assurance Notes :Acceptance Criteria:Yes No N/AA . Holding Time :Allcriteriamet .All criteria met .B . Surrogates :All criteria met .El 0714 days from sample collection forTCLP extraction .14 days from sample collection(or TCLP extraction) for analysis .® F-1 50% - 150% RecoveryC. Notes :I certify that except as specifically noted in this report , all statements and data appearing in this report are in conformancewith the provisions of the Quality Assurance Plan (QA P) prepared by this firm and on file with the Alaska Department ofEnvironmentalConservation,/ /Analyst' s Signature :Printed Name & Date : G race S . MarianoReviewer 's Signature :8/13/97Printed Name & Date :Volatiles Quality Control Summanf PageCT&E Environmental Services Inc .:.DeliverablesQA/QC Data8/13/97Analysis Date :Analysis Lot Number:VDA06060813Aromatic Volatile Organics / Gasoline Range OrganicsAnalysis :Method: BTEX by EPA 8020/602/AK101 ( 8015M)Solid/LiquidMatrix:Analysis :Assurance Notes :Acceptance Criteria :Yes NoA.Calibration :All criteria met .QB.Method Blank:All criteria met .0 F7C . Continuing Calibration Verification Std :0All concentrations are below thePractical Quantitation LimitD.Laboratory Standard :All criteria met.0RF 14 .00 _~H12 .00_10 .00Ia2 .000 .00 -102. 04 .4006.Minutes8.010 .00ISampleName IS Acq Meth Set VDA _Mth_Set Dilution 1 .000Analysis_Lot VDA06060813 Date Acquired 08/13/97 09 :13 :53 PM SampleWeight 1 .000Prep _Lot 0813VH01 Processing Method VDA_FID _ 0624 Initials GSMChannel Descr . FIDVPH Results#1234NameSurrogateHexaneGRODifluorobenzene5aaa -TFT6'4-Bromofluorobenzene7Ret Time(min)Decane2 .682 .684 .675 .42Area(uV* sec)2915701612298497114468114148- 8-.66629 5 -59 .41415SlnConcSur_Rec_1( $ )Sur Rec 2( % )-True GRO128 .473 .052131 .523 .0523 .05235 .2588 .13 .05245 .18--j-j.5979 .03 .0523 .0523 .052SampleName : IB Analysis Lot : VDA06060813 Prep Lot : 0813VH01Date Acquired : 08/13 / 97 09 : 13 :53 PM Channel Descr . : PID Dilution : 1 .00000S ampleWeight : 1 . 00000 Initials : GSM120 .00 .-1110 . 00_-I100 .00_190 .00 80 .0070 .00 60 .00 ,50 .00 -I0.02.04.06.0Minutes8.010 .00SampleName 1B Acq Meth Set VDA _Mth_SetDilution 1 .000Analysis_Lot VDA06060813Date Acquired 08/13 / 97 09 : 13 :53 PM SampleWeight 1 .000Prep Lot 0813V1401Processing Method VDA_PID_0606 Initials GSMChannel Descr . PIDResults#NameRet Time(min)11,4-Difluorobenzene4 .672aaa-TFT5 .423P & M -Xylene4-Bromofluorobenzene8 .0748 .66Area(uV*sec )157875164653SlnConc38 .001 .00Amount( PPB )37 .9971 .00011150 .130 .12630094637 .7437 .742Sur _Rec_1( )Sur_Rec_2(-I- )95 .094 .4SampleName : CCV2 Analysis _Lots VDA06060813 Prep Lot : 0813VH01Date Acquired : 08/13 / 97 09 :33 : 53 PM Channel Des,cr . : PID Diluti on : 1 .00000Sampleweight : 1 .00000 Initials : GSM110 .00-1AU,100 .00_1- j0HqasNe90 .00 _j14yU)v80 .00 -_13mymN~A 70 .00 _OHm60 .00mNqmAa.040N10MNAba 04MinviV40 .00mmOwMNn0~u1ribwmOin130 .0020 .0010 .00 _~ILUUL0 .00 _-10. 02A O4. 06 .40Minutes8.010!0SampleName CCV2Acq Meth Set VDA_Mth_Set Dilution 1 .000Analysis _ Lot VDA06060813 Date Acquired 08/13 / 97 09 :33 :53 PM SampleWeight 1 .000Prep Lot 0813VH01 Processing Method VDA_PID _ 0606 Initials GSMChannel Descr . PIDResults#NameRet Time(min)Area(uV*sec)SlnConcAmount( PPB )1Benzene4 .2521,4-Difluorobenzene20152419 .7119 .7084 .6715177336 .381653121835481 .0036 .3833 aaa - TFT4 Toluene5 Ethylbenzene678P & M -XyleneO -Xylene4-Bromofluorobenzene5 .426 .537 .908 .078 .378 .6615786836711616310229445019 .7019 .841 .000Sur_Rec _ 1( )Sur_Rec_2(-I; )91 .019 .70119 .84441 .2441 .24420 .1336 .7836 .78020 .13491 .9SampleName : CCV Analysis Lott VDA06060813 Prep Lot : 0813VH01Date Acquired : 08/13/99 09 :54 :24 PM Channel Descr . : FID Dilution : 1 .00000SampleWeight : 1 .00000 Initials : GSM30 .00--I8,amab0a:12 .00 -LL0 .000 .0_,V LLL_2.L_L0_L_ ___4.uv,Uv'vL L -L0~v tLLLL1LL6.0MinutesLIt8.U IN 1 .1 VVL. 11 .L ILL _LLLL ILL L. LLL Lt .I010 .00SampleName CCV Acq Meth Set VDA_Mth_Set Dilution 1 .000Analysis_Lot VDA06060813 Date Acquired 08/13/97 09 :54 :24 PMSampleWeight 1 .000Prep Lot 0813VH01 Processing Method VDA_FID_0624 Initials GSMChannel Descr . FIDVPH Results#123NameSurrogate'HexaneGRORet Time(min)140 .262 .68782404344 .7411934836 .7612660850 .118 .66723639 .401002136 .31Difluorobenzene4 .6755 s--TFT5 .424-Bromofluorobenzene7 DecaneSlnConc3183192 .6846Area(uV * sec)26971Sur Rec _ 1Sur_Rec_2True GRO204 .485204 .485204 .48591 .9204 .485204 .48590 .8204 .485204 .485SampleName : QC Analysis Lot : VDA06060813 Prep Lot : 0813VH01Date Acquired : 08/13 / 97 10 :14 : 31 PM Channel Descr . : FID Dilution :SampleWeight : 1 .00000 Initials : GSM1 .00000180 .00 . .160 .00140 .00120 .00-100 .00-mOidxwxOmt0I80 .0060 .0040 .0020 .00'f~ 110 .02.11 1~ 1111 11 11 ~04.06.0Minutes8.01'0 .00SampleName QCAnalysis _ Lot VDA06060813Prep_Lot 0813VH01Channel Descr . FIDAcq Meth Set VDA_Mth_SetDate Acquired 08/13 / 97 10 : 14 :31 PMProcessing Method VDA_FID_0624Dilution 1 .000SampleWeight 1 .000Initials GSMVPH ResultsName#12SurrogateHexane3 GRO4 Difluorobenzene5 aaa-TFT674-BromofluorobenzeneDecaneRet Time(min)2 .68Area(uV*sec)SlnConc316796521880139 .5911675335 .962 .684 .6724335161072 .265 .4213142252 .028 .669 .406862249149034 .43Sur Rec_ 1()Sur Rec_2Ft- )True GRO932 .669932 .669932 .669932 .66989 .986 .1932 .669932 .669932 .66932 .00SampleName : 113552 Analysis Lot : VDA06060813 Prep Lots 0813VS01Date Acquired : 08/14/97 03 : 44x22 PMChannel Descr . : FID Dilution : 1 .00000SampleWeight : 1 .00000 Initials : GSM30 .0028 .0026 .0024 .0022 .0020 .0018 .00H16 . 0014 .0012 .0010 .008 .006 .004 .00IAA2 .00nT2. 04 .406. 0MinutesV ------T10 .00TATSampleName113552Analysis_Lot VDA06060813Prep _Lot 0813VS01Channel Descr . FIDAcq Meth Set VDA_Mth_SetDate Acquired 08/14 /97 03 : 44 :22 PMProcessing Method VDA_FID_0624Dilution 1 .000SampleWeight 1 .000Initials GSMVPH Results#123NameSurrogateHexaneGRO4 DifluorobenzeneRet Time(min)2 .692 .69Area(uV*sec)3097882494SlnConc326049117789143 .6636 .285 .4312715550 .3332 .54aaa-TFT64-S romofluorobenzene8 .67648457Decane9 .421359Sur Rec 2( % )136 .504 .685Sur_ Rec_1( % )True GRO-7 .1657 .1657 .1657 .16590 .77 .16581 .37 .1657 .165SampleName : 113552 Analysis Lot : VDA06060813 Prep Lot : 0813VS01Date Acquired : 08/14/97 03 :44 :22 PM Channel Descr . : PID Dilution : 1 .00000SampleWeight : 1 .00000 Initials : GSM100 .00_90 .0080 .00 -70 .00 -:s 60 .00 50 .00 -I40 .00 30 .0020 .00 10 .000 .000 .00T2 .006 .40MinutesIio .ooTSampleName 113552 Acq Meth Set VDA_Mth_Set Dilution 1 .000Analysis Lot VDA06060813 Date Acquired 08/14/97 03 :44 :22 PM SampleWeight 1 .000Prep _Lot 0813VS01 Processing Method VDA_PID_0606 Initials GSMChannel Descr . PIDResultsNameRet Time(min)11,4-Difluorobenzene4 .6823aaa-TFTToluene5 .436 .554P & M -Xylene8 .08#54-Bromofluorobenzene8 .67Area(uV* sec)16177118225720351708305804SlnConc35 .171 .000 .200 .1734 .65Amount( PPB )35 .1741 .0000 .198Sur Rec_ 1( )Sur Rec_2(-%- )87 .90 .17434 .64786 .6SampleName : LS Analysis Lot : VDA06060813 Prep Lot : 0813VS01Date Acqui red : 08/14 /97SampleWeig ht : 1 .0000004 : 04 :55 PM Channel Descr . : FID Dilution : 1 .00000I nitials : GSM30 .0028 .0026 .0024 .00 .22 .00 -20 .0018 . 00>FmromKx16 . 00 _N14 .00 .--N12 .00 _I10 .00-8 .00II-6 .00 -IUm4 .002 .00_i1; 1L`-L_L_L_-ION ~ H~k. W1k -1 X . "W,L _LL _ LL _LLL LL LL _LLL LLPL L -1.1-1-0 .00 -0 .80-2.04A06.0Minutesa.o10 .00M-ASampleName LS Acq Meth Set VDA_Mth_Set Dilution 1 .000Analysis _Lot VDA06060813 Date Acquired 08/14 /97 04 : 04 :55 PMSampleWeight 1 .000Prep_Lot 0813VS01 Processing Method VDA_FID_0624 Initials GSMChannel Descr . FIDVPH Results#NameRet Time(min)Area(uV*sec)344546SinConc1Surrogate2Hexane2 .70684563GRO2 .7022867474 .6914721945 .34True-GRO855 .772855 .7721007 .59Dfluorobenzene5aaa-TFT5 .4412238348 .4464-Bromofluorobenzene8 .677494437 .619 .511089DecaneSur_Rec_2( )151 .8147Sur_Rec-1( % )855 .7'72113 .4855 .772855 .77294 .0855 .772855 .772SampleName : LS Analysis_ Lot : VDA06060813Prep Lot : 0813VS01Date Acquired : 08/14 / 97 04 : 04 :55 PM Channel Descr . : PID Dilution : 1 .00000SampleWeight : 1 .00000 Initials : GSM450 .00400 .00-350 .00-'m300 .00--mN[ZmAAONwOH250 .00- .0v200 .00--lmmIIq41A150 .00__®N iOmII,qNSEeNt,00w00QmmNoO t-rn0Co- .~ ~ II ~Il~~ . w100 .00_'Nd~AVLn50 .00 --L--J0 .002. 04. 0l_ ___ II UUL1UA,_ .6.0Minutes8.~-- r-- -~---~ _ _-f--- --010 .00SampleName LS Acq Meth Set VDA_Mth_Set Dilution 1 .000Analysis _Lot VDA06060813 Date Acquired 08/14/97 04 : 04 :55 PMSampleWeight 1 .000Prep_Lot 0813VS01 Processing Method VDA_PID_0606 Initials GSMChannel Descr . PIDResultsName#1BenzeneRet Time( min)4 .28Area(uV * sec)40549836 .4036 .39721,4-Difluorobenzene4Toluene6 .551426640140 .54140 .5435Ethylbenzene7 .9121315424 .5924 .592670 -Xylene8 .388 .6729598734052333 .5439 .0433 .53639 .040aaa-TFTP & M -Xylene8 4-Bromofluorobenzene5 .448 .0818011084981940 .82Amount( PPS )4 .693185540SlnConc1 .0087 .6340 .823Sur_Rec_1( % )Sur_Rec_2( % )102 .11 .00087 .63097 .6SampleName : 113553 Analysis Lot : VDA06060813 Prep Lot : 0814VH01Date Acquired : 08/14/97 05 :27 :16 PM Channel Descr . : FID Dilution : 1 .00000SampleWeight : 1 .00000 Initials : GSM30 .00_28 .0026 .00_24 .0022 .0020 .00_18 .00__16 .00_14 .0012 .0010 .008 .00I6 .00im4 .00 -U2 .00J0 .00V ~-L _ L2.U _W _0_ L_ L4.:L-V0-LV\4 LL _6. 0Minutes-_>I 11 L IV Vii _LL Q L V8. 0L:LW W U~0 .00A1SampleName 113553Acq Meth Set VDA_Mth_Set Dilution 1 .000Analysis-Lot VDA06060813 Date Acquired 08/14 / 97 05 :27 :16 PM SampleWeight 1 .000Prep_ Lot 0814VH01 Processing Method VDA FID- 0624 Initials GSMChannel Descr . FIDVPH Results412345NameSurrogateHexaneGRO5ifluorobenzeneaaa-TFT6 4-BromofluorobenzenejDecaneRet Time(min)2 .712 .71Area(uV*sec )32865972152SlnConc144 .814 .702266583142619998 .7043 .925 .4511345444 . 919 .518198 .6872586Sur Rec_1( W )36 .42Sur Rec-2( 1True GRO853 .888853.888853 .888853 .888109 .891 .1853 .888853 .899853 .888SampleName : 113553 Analysis Lott VDA06060813 Prep Lot : 0814VH01Date Acquired : 08/14/97 05127 :16 PM Channel Descr . : PID Dilution : 1 .00000SampleWeight : 1 .00000 Initials : GSM440 .00---mqw420 .00k400 .00380 .00--wa360 . 00_CO340 .00_0320 .00300 .00_mAmN280 .00_C!260 . 00_WA0nH0N240 .00--H.-1N220 .00-wvmd200 . 00180 . 000mN160 .00-t;mNA?C '.[COMWCD Imm140 .00N120 .00-100 .00-1M80 .00 _tV60 .00 _adO0r1WrIArlO0nm offD om NVO:ANOtabwIInA ~ 1 1 111111 A I40 . 00 _l20 .000 . 00-20 .00_0 .00F-T 2. 04. 06 .40MinuteseTo10 .00T--1-_TSampleName 113553 AcqAnalysis Lot VDA06060813Prep _Lot 0814VH01Channel Descr . PIDMeth Set VDA_Mth _ Set Dilution 1 .000Date Acquired 08/14 / 97 05 : 27 :16 PM SampleWeight 1 .000Processing Method VDA_ PID_0606 Initials GSMResults9Name1Benzene21,4-Difluorobenzene345aaa-TFTTolueneEthylbenzene6 -- V& M -Xylene78O -Xylene4-BromofluorobenzeneRet Time(min)4 .294 .705 .45Area(uV*sec)404813SlnConc38 .8917907642 .181682581 .00Amount( PPB )38 .89542 .1761 .0006 .5514124987 .92148 .95148 .95221286026 .2926 .2888 .098 .388 .6885088029577633247193 .9235 .8740 .80Sur_Rec_I(%)Sur_Rec_2(% )105 .493 .92035 .87340 .802102 .0SampleName : 113554 Analysis Lot : VDA06060813 Prep Lot : 0814VH01Date Acquired : 08/14/97 05 :47 :49 PM Channel Descr . : FID Dilution : 1 .00000SampleWeigh t : 1 .0000 0 In itials : GSMA1Iv~V VI 10 .00 -10 .602 . b0-U-Q v4 .40aI6 .40wL f. 11L L _ ILL _Minutes11_'IL8 .00U U L l1 _LLL LI I10 .00SampleName 113554Acq Meth Set VDA_Mth_ Set Dilution 1 .000Analysis-Lot VDA06060813Date Acquired 08/14 / 97 05 :47 :49 PM SampleWeight 1 .000Prep_Lot 0814VH 01 Processing Method VDA_FID _ 0624 Initials GSMChannel Descr . FIDVPH Results#NameRet Time(min)Area(uV * sec)ISurrogate2Hexane2 .72705313GRO2 .7222212204 .721358844Difluorobenzene5aaa-TFT64-Bromofiuorobenzene7 -De-cane----3145145 .461081518 .69704799 .521363SlnConcSur Rec_1()Sur Rec_2( )138 .58True GRO840 .132840 .132978 .7141 .8542 .8135 .37840 .132104 .6840 .132840 .13288 .4840 .132840 .132SampleName : 113554Analysis _Lott VDA06060813 Prep Lots 0814VH01Date Acquired : 08/14 / 97 05 : 47 :49 PM Channel Deecr . : PID Dilution : 1 .00000SampleWeight : 1 .0000 0 Initials : GSM440 .00_420 .00400 .00380 .00_360 .00-J340 .00320 .00300 .00 1280 .00260 .00_240 .00_220 .00200 .00-180 .00160 . 00140 .00-120 .00-100 .00-80 .0060 .0040 .00 __20 .000 .00-20 .000.02 .404.06.Minutes08 .0010 .00SampleName 113554 Acq Meth Set VDA_Mth_Set Dilution 1 .000Analysis-Lot VDA06060813 Date Acquired 08/14/97 05 :47 : 49 PMSampleWeight 1 .000Prep_Lot 0814VP01 Processing Method VDA_PID_0606 Initials GSMChannel Descr . PIDResults#Name1Benzene3aaa-TFT21,4-Difluorobenzene4Toluene5Ethylbenzene6178P & M -Xylene0 -Xylene4-BromofluorobenzeneRet Time(min)4 .314 .725 .466 .567 .938 .108 .398 .69Area(uV*sec)SinConc40266639 .981628151 .00171600140315821080984371429404832119341 .77Amount( PPS )Sur_Rec_2( )39 .98241 .7661 .000152 .91152 .91396 .2496 .24226 .90Sur_Rec_1(-%- )104 .426 .90436 .8636 .85540 .7440 .736101 .8SampleName : 974607001 Analysis Lot : VDA06060813 Prep Lot : 0814VH01Date Acquired : 08/14 / 97 06 :07 :56 PM Channel Descr . : FID Dilution : 1 .00000SampleWeight : 1 .00000 Initials : GSM28 .00_26 .00- -~24 .0022 .00_20 .00-118 .0016 . 00 --~12 . 00 710 .008 .00 6 .00-I4 .00 -1maro14x1I1C2 .00 -10 .000 .002. 04.06.0Minutes8.010, .00SampleName 974607001 Acq Meth Set VDA_Mth_Set Dilution 1 .000Analysis Lot VDA06060813 Date Acquired 08/14 / 97 06 :07 :56 PM SampleWeight 1 .000Prep Lot 0814VH01Processing Method VDA_ FID_0624 Initials GSMChannel Descr . FIDVPH Results#NameRet Time(min)Area(uV*sec)1Surrogate2Hexane2 .712414GRODifluorobenzene2 .714 .713155251110605aaa-TFT5 .4612057047 .7264-Bromofluorobenzene8 .696348531 .867Decane9 .53109034295115SlnConcSur Rec_1( 9 )Sur Rec 2! )130 .03True GRO8 .9938 .993139 .0334 .218 .993 .8 .99385 .58 .99379 .68 .9938 .993SampleName : 974607001 Analysis _Lot : VDA06060813 Prep Lot : 0814VH01Date Acquired : 08/14 / 97 06 : 07 :56 PM Channel Descr . : PID Dilution : 1 .00000SampleWeight : 1 .00000 Initials : GSM120 .000110 .000100 .00A90 .00H}~N80 .00v70 .00mqHqm60 .00pN0briIdw,qnLn50 .00Hmn40 .00HLn1'30 .0020 .0010 .000 .000.02.04. 06 .40Minutes8 .4010 .00SampleName 974607001 Acq Meth Set VDA_Mth_Set Dilution 1 .000Analysis Lot VDA06060813 Date Acquired 08/14 /97 06 : 07 :56 PM SampleWeight 1 .000Prep Lot 0814VH01Processing Method VDA_PID_0606 Initials GSMChannel Descr . PIDResults#NameRet Time(min)Area(uV * sec)SinConcAmount( PPB )11,4-Difluorobenzene4 .7115958235 .2535 .2472aaa-TFT5 .461794161 .001 .0003Toluene6 .5725180 .250 .2494P & M -Xylene8 .10240650 -Xylene0 .250 .2498 .4012960 .150 .14764-Bromofluorobenzene8 .6930732435 .3735 .370Sur_Rec_1(-%- )Sur_Rec_2(-%- )88 .188 .4SampleName : 974607002 Analysis Lot : VDA06060813 Prep Lot : 0814VH01Date Acquired : 08/14 / 97 06 : 27 :58 PM Channel Descr . : FID Dilution : 1 .00000SampleWeight : 1 .00000 Initials : GSM28 .0026 .0024 .0022 .0020 .0018 .00-116 .00 7AS 14 .00-~!Da12 .00-110 .00--~8 .00 -6 .00 4 .00I~2 .00 -a0 .00 -a0.\)11--02 . 0A-I-4A O6.0Minutes8.010 .'00SampleName 974607002 Acq Meth Set VDA_Mth_Set Dilution 1 .000Analysis Lot VDA06060813 Date Acquired 08/14/97 06 :27 :58 PM SampleWeight 1 .000Prep_Lot 0814VH01 Processing Method VDA_FID_0624 Initials GSMChannel Descr . FIDVPH Results#NameRet Time(min)Area(uV * sec)1SurrogateHexane2 .71167613GRO2 .71Difluorobenzene4 .72321934141 .8512020164-Bromofluorobenzene47 .5878 .696210831 .16Decane9 .53975245aaa-TFT292660SlnConc5 .46110351Sur Rec_1( t )Sur Rec 2( )128 .9533 .99True GRO-12 .89912 .89912 .89985 .012 .89977 .912 .89912 .89912 .899130 .001SampleName : 974607002 Analysis Lot : VDA06060813 Prep Lot : 0814VH01Date Acquired : 08/14/97 06 :. 27 :58 PMChannel Descr . : PID Dilution : 1 .00000SampleWeight : 1 .00000 Initials : GSM120 .00p110 .00-)100 .0090 .00 -]80 .0070 .00 R 60 .0050 .00 40 .0030 .00 720 .0010 .000 .002 .404. 06 .40Minutes8 .40101.00SampleName 974607002 Acq Meth Set VDA_Mth _Set Dilution 1 .000Analysis Lot VDA06060813 Date Acquired 08/14 / 97 06 : 27 :58 PM SampleWeight 1 .000Prep_Lot 0814VH01 Processing Method VDA _PID_0606 Initials GSMChannel Descr . PIDResults#NameRet Time(min)Area(uV*sec)SlnConcAmount( PPB )1,4-Difluorobenzene4 .7215889535 .2235 .2232aaa - TFT5 .461787681 .001 .0003Toluene6 .5711740 .120 .11754-Bromofluorobenzene8 .118 .6911063051070 .1135 .240 .11535 .24214P & M -XyleneSur Rec_1( )Sur Rec 2( )88 .188 .1SampleName : LS Analysis Lot : VDA06060813 prep Lot : 0814VH01Date Acquired : 08/14/97 09 :28 : 29 PM Channe l Descr . : FID Dilution :Samp leWeight : 1 .00000 Initials : GSM1 .00000ISNIIAIISampleName LS Acq Meth Set VDA_Mth_Set Dilution 1 .000Analysis Lot VDA06060813 Date Acquired 08/14/97 09 : 28 :29 PMSampleWeight 1 .000Prep_Lot 0814VH01 Processing Method VDA_PID _0624Initials GSMChannel Descr . FIDVPH Results#1NameSurrogateRet Time(min)Area(uV*sec)HexaneGRO2 .734Difluorobenzene2 .73333986706502229792S4 .73143381aaa-TFT5 .474-DromofluorobenzeneDecane8 .699 .531172612367733441271SlnConcSur_Rec_1Sur_Rec_2147 .16982 .4944 .1646 .4136 .80True-GR0835 .330835 .330835 .330110 .4835 .33092 .0835 .330835 .330835 .330SampleName : LS Analysis Lot : VDA06060813 Prep Lot : 0814VH01Date Acquired : 08/14 / 97 09 : 28 :29 PM Channel Descr . : PID Dilution : 1 .00000Sampleweight : 1 .00000 Initials : GSM450 .00 .E400 .00-350 .00300 .00-A250 .00-II200 .00-111 f"I am150 .00-JIn,°4HE+ I)an100 . 00__1M.-11'A M50 .00 -JOmMIIIN:111IInOdlh0 .000.02 .404. 06 .40Minutes8. 0f.10 .00SampleName LSAcq Meth Set VDA Mth Set Dilution 1 .000Analysis _ Lot VDA06060813 Date Acquired 08/14/97 09 :28 :29 PM SampleWeight 1 .000Prep Lot 0814VH01 Processing Method VDA_PID_0606 Initials GSMChannel Descr . PIDResults#NameRet Time(min)12Benzene1,4-Difluorobenzene4 .33345678aaa - TFTTolueneEthylbenzeneP & M -Xylene0 -Xylene4-Bromofluorobenzene4 .735 .476 .577 .938 .108 .408 .69Area(uV*sec )4063321858581781251431793213993855500298203340491SlnConc36 .8841 .351 .00142 .6224 .9689 .2034 .1639 .47Amount( PPS )36 .87841 .3481 .000Sur_Rec 1( %) -Sur Rec 2(_g )-103 .4142 .62224 .96389 .19934 .16339 .47298 .7Semi -Volatiles. :Sample :QC Summary Page ::Cl'&E: Environmental Services Inc .QA/QC Data DeliverablesWorkorder Number :Analysis Lot Number :sfReizzagilrExtraction Lot Number.XX)( 3/2 011 Y-1-19 ;IAnalysis : Diesel Range Organics/Residual Range OrganicsMethod : AKI02/103Matrix : LiquidAnalysis:Assurance Notes :Acceptance Criteria:Yes No N/AA . Bolding Time :All criteria met .All criteria met.All criteria met.B.Surrogates :All criteria met.Q14 days from sample collection forTCLP extraction.14 days from sample collection (or7 days from TCLP extraction) forprep extraction.40 days from extraction for analysis.50% - 150% RecoveryC . Notes :I certify that except as specifically noted in this report, all statements and data appearing in this report are in conformanceWith the provisions of the Quality Assurance Plan (QAP) prepared by this firm and on file with the Alaska Department of ,Environmental Conservation .Analyst's Signature :. Date :Printed Name .&Reviewer' s Signature:/~=9~Printed Name & Date :-/ r'~ fSemi-Volatiles Quality Control Summary PageCr&E Enviranmental::Services Inc.I QA/QC*Data Deliverables .Analysis Date :..g / y q 0Analysis Lot Number:Extraction Lot NumberAnalysis:Diesel Range Organics/Residual Range OrganicsMethod : AK102/103Matrix:LiquidAssurance Notes :Analysis:YesC/ZLodF/f20Acceptance Criteria :No'A.Calibration :All criteria met.B.Method Blank:All criteria met.All concentrations arc below thePractical Quantitation LimitC.Continuing Calibration Verification Std :All criteria met .IO .995 .Relative Standard Deviation Staraard10Standard01/22 9719 :03 :1101 ;22,9701/22 / 97'_3 :42 :0612Standard19 :53 :4215Standard01/22/ 9701/22 / 97 21 : 17 :2411Standard13Standard161Standard181921222324252728293031StanarStandardStandard; StandardStandardStandardStandardStandardStandardStandardStandardStandardStandard19 :20 :59SATINSCR01220_22SATIN-2SCR01220122SATIN-2SCRO1220122SATIN-2SATIN-2SATIN-201/22 / 97 21 :56 :12 SATIN - 20/29 2 : 4 :5 SATIN 01/22 / 97 23 : 13 :36 SATIN-201 /22/97 23 :52 :16 SATIN-201 /23/97 01 :09 :43 SATIN-201/23/97 01 : 48 :13 SATIN - 201 /23/97 02 :27 :04 ; SATIN-201 /23/97 03 : 05 :38 SATIN-201 /23/97 03 :44 : 341 SATIN-201 723/97 05 :02 : 01 ; SATIN-201/ 23/97 05 :40 :44 SATIN-2~ 01/ 23/97 06 :19 : 24 1 SATIN-201 /23/97 06 :58 :2 5 SATIN - 27 07-.3- -7 :30 SATIN-20172--3T9-SCRO1220122SCRO1220122SCR01220122SCR01220122SCR01220122SCRO1220122SCRO1220122SCR01220122SCRO1220122SCRO1220122SCRO1220122! SCRO1220122SCRO1220122SCRO1220122SCRO1220122SCRO1220122SCR01220122Analysis-Lot-R : SCRO1220814 _ SampleName . . C10-C44 Prep Lot-R :0814EB01N140 .00_120 .00 100 .00-JO80 .00 --60 .00 -p0 .d0-5 .0015 .00MinutesJLJ~--T20 .0025 .00Channel Descr . Rear _ FIDSampleNameR C10-C44Acq Meth Set SC AK102 AK103Analysis Lot R SCRO1220814Date Acquired 08/14/97 03 : 40 :40 PMPrep Lot R 0814EB01Processing Method SCR AK102 AK103S _ 0122 MI- r 3 R 0 .0000Dilution -R1 .00000SampleWeightR 1 . 00000Initials WAASurr 4 R 0 .0000DRO and RRO Results#NameRet Time(min)Area(uV * sec)Sln Conc-TRUERRO-RTrueDiesel_R1SURROGATE AK10224142SURROGATE AK1031 .6441964 .7428Diesel2 .0734126 .37143407012 .573104033311964 .74285 alpha Androst5C2415 .773414217 .8001 .3871964 .74284126 .371444128 .0156RRO2920682718 .7203861840DTC20 .2001966 .8151964 .74288C3640701 .62122 .5079288121964 .74284126 .37141964 .74284126 .3714y4126 .37141964 .74284126 .37141964 .74284126 .37144126 .3714Analysis Lot R :SCRO1220814SampleNamek :CCVB 12500Prep-Lot-R :0814EB01200 . 00180 .00_160 .00-1140 .00__120 .00Mu0L0 .00-----------------------%0l0C4.i10 .0015 .00Minutes00I1TI--125 .00TChannel Descr . Rear _FID SampleNameR CCVB 12500 Dilution -R 1 .00000Acq Meth Set SC _AK102_AK103 Analysis _Lot_R SCRO1220814SampleWeightR 1 .00000Date Acquired 08/14/97 04 :18 :06 PM Prep Lot R 0814EB01 Initials WAAProcessing Method SCR AK102 AK103S_01225Ri1-r 3 R 0 .0000Surr 4 R 0 .0000DRO and RRO ResultsRet Time(min)4Name1SURROGATE AK1022SURROGATE AK103j3Diesel45 alpha Androst5C256RRO7DTC8C361Area(uV * sec)TRUERRO-R12229537 7048 .526120 .981511 .0171 .9203328388715 .77313206 .960120 .981512229540 .944--- -18 . -1 306569518 .130_Sln- Conc241317122 .901---20--.247 - --3 7701 .50122 .660171852120 .9815120 .9815120 .9815120 .9815120 .9815120 .9815TrueDiesel-R13158 .434013158 .434013158 .434013158 .434013158 .434013158 .434013158 .434013158 .4340Analysis-Lot-R :SCRO122O814S ampleNamei. . SFIB 100/100 Prep Lot R : O814EB01_280 .00_UNA260 .00-nin240 . 00 _160 .00 7140 .00-120 .00_;100 .0080 .0060 .00 40 .00 -120 .00 -111-0 .000 .00ir5 .010 .0015 .00Minutes20 .0025 .00Channel Descr . Rear _ FIDSampleNameR SFIB 100 / 100Acq Meth Set SC_AK102 _AK103Analysis Lot R SCRO1220814Date Acquired 08/14 / 97 04 : 55 :37 PMPrep_ Lot R 0814EB01Processing Method SCR_AK102_AK103S_0122_SRi '1-r_3_R 100 .0000Surr 4 R 100 .0000Dilution -R 1 .00000SampleWeightR 1 .00000Initials WAADRO and RRO ResultsRet Time(min)Area(uv * sec)#Name1SURROGATE AK1023300382SURROGATE AK103130 .9583Diesel450174229 .271501940199 .16947 .977Sln Conc-5 alpha Androst15 .7705C2819 .7436RRO62968719 .743707816360 .487DTC20 .1574501748C3622 .893179 .26230102330038110 .497Surr(~Rec _3)Surr Rec_ 4(%)TRUERRO-R131 .215668 .2105131 .215668 .2105131 .2156110 .497131 .2156179 .262TrueDiesel_R68 .210568 .2105131 .215668 .2105131 .215668 .2105131 .215668 .2105131 .215668 .2105Analysis L ot R : SCRO1220814SampleName _ . CCVR 10000 Prep Lot R :, 0814EB0 1280 .00-260 .00 .1240 .00--_220 .00200 .00-y180 .00_160 .00140 .00-A!120 .00--100 .0080 .00 -60 .0040 .00 -20 .00 0 .000.TTT05. 0Ir 15 .00Minutesr 20 .0025 .00Channel Descr . Rear FIDSampleNameR CCVR 10000Acq Meth Set SC AK102 AK103Analysis Lot R SCRO1220814Date Acquired 08/14 / 97 05 : 33 :11 PMPrep Lot_R 0814EB01Processing Method SCR AK102 AK103S_0122j'?r 3 R 0 .0000Surr 4 R 0 .0000Dilution- R 1 .00000SampleWeightR 1 . 00000Initials WAADRO and RRO Results#NameRet Time(min)1SURROGATE AK1032SURROGATE AK1023Diesel415 .6975 alpha Androst5C256RRO7DTC8C36 -Area(uV * sec)533552Sln Conc-TRUE-RRO-RTrueDiesel-R271 .73510472 .217710 .2451668 .8775423168810472 .21771668 .877515 .8031679 .12310472 .2177258208 .6451668 .877518 .127321821810472 .21771668 .877520 .04010472 .2177210957411668 .877520 .24310743 .95310472 .2177533552212 .4641668 .8 77510472 .21771668 .877510472 .21771668 .877525820____22 .66783552Analysis Lot R : SCRO1220814SampleNamer >_ LSB 8000 Prep_Lot_R : 0814EB01480 .00__7460 .00440 .00 420 .00400 .00 :_380 .00_ .360 .00__340 .00320 .00:300 .00280 .00 ::0140 .00120 .00100 .0080 .0060 .0040 .0020 .00 0 .000 .005. 0r10 .0015 .00MinutesT20 .0025 .00Channel Descr . Rear-FIDAcq Meth SetSCDate AcquiredAK102SampleNameRAK10308/15 / 97 02 : 17 :52LSBAnalysisLotRAMLotRPrep8000DilutionSCRO12208140814EB01InitialsDRO RearArea(uV*sec)#Name1SURROGATE AK10227055627 .996SURROGATE AK1038799 .55883Diesel33201 .6918799 .5588410 .990222470088827 .5555 alpha Androst15 .780705568799 .558818 .1305709723 .6228799 .55885C256RRO78Sln Conc-18 .130DTC18561894 .53420 .23033201 .322C3622 .6531252021 .000000SampleWeightRProcessing Method SCR AK102 AK103S - 0122 R7 Surr_3 R 0 .0Ret Time(min)RTrue Diesel R-8799 .55888799 .55888799 .55888799 .5588WAA1 .00000A a_lvsi. s _Lot-T-i-R_ !SS_R_ O1__22_ 0814_Sampl eNamek :LSB 8nnn Pr ep L ot R :0 814ER0'1480 .00460 .00_440 .00420 .00--400 .00--380 .00 "360 .00340 .00320 .00300 .00=280 .00_260 .00_240 .00_220 .00--.200 .00180 .00-1160 .00_140 .00120 .00_100 .00 _80 .00In60 .00 _-40 .00 120 .00 00 .00 -10 .00•14AOM10 .0015 .00Minutesto%DO20 .00MUO%0MrqNn00L------------------------------ '45 .00UNUTNI25 00Channel Descr .AcqMethSetRearSC_FIDAK102SampleNameRAK103Date Acquired 08/15/97 09 :29 :20AMAnalysisPrepLSBLotLotRR8000DilutionSCRO12208140814EB01RSampleWeightRInitialsWAAProcessing Method SCR AK102 AK103S-0122 R7 Surr_3 R 1 .0DRO RearRet Time(min)Area(uV*sec)#Name1SURROGATE AK102391282SURROGATE AK10315 .5263Diesel5 alpha Androst25601 .30445 C256RRO7DTC8 C3610.987Sin Conc-15 .83021811003391288654 .54918 .16014567374 .19120 .23325601 .01918 .16022 .660495449357013 .100Surr R'c_3aTrue Diesel R8639 .02358639 .02351310 .01 .0000008639 .02358639 .02358639 .02358639 .02358639 .02358639 .02351 .00000Analys is-L ot R : SCRO1220814 S ampleNamek .BLK 3120 Prep Lot R ®XXX310445 .00 . .40 .00 _135 .00-30 .0025 .00_20 .00 .InNU15 .00%0mUMa,1'10 .00_1wQ- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ~'- - - - - - - - - - - - - - - I5 .00b0 .00-5 .00-- 0InUHqhMIn.05 .6010 .0015 .00MinutesinON20 .00I25 .00~SampleNameR BLK 3120Channel Descr . Rear_ FIDAnalysis Lot R SCRO1220814Acq Meth Set SC _AK102 AK103Date Acquired 08/15 / 97 11 : 24 :41 AMPrep Lot R XXX3104Processing Method SCR AK102 AK103S _ 0122 M'_-r 3 R 100 .0000Surr 4 R 100 .0000Dilution R 1 .00000SampleWeightR 1 .00000Initials WAADRO and RRO ResultsRet Time(min)Area(uV * sec)Sin Conc-Surr Rec-3Surr Rec_4J)Name1SURROGATE AK10225162599 .84486 .860974 .97992SURROGATE AK103232023118 .16886 .860974 .97993Diesel440588- i5 .720 - -174 .82486 .860974 .9799-i5 --alpha Androst86 .860974 .97995C2515 .75718 .4932516254793984 .2446RRO88 .493402574205 .0297DTC20 .13323202392 .3938C3622 .693332884 .244TRUE RRO R- -86 .860986 .860992 .39386 .860986 .8609True Diesel R-74 .979974 .979974 .979974 .9799Analysis-Lot-R :SCRO1220814SampleName , . . LCS 3120 Prep LotR : XXX31O4280 .00 __260 .00- .240 .00--A'220 .00200 .00in180 .00'160 .00-140 . 00__120 .00--100 .0080 .00._j60 .00 _-0 .005.010 .0015 .00Minutesr20 .00T25 .00Channel Descr . Rear _ FID SampleNameR LCS 3120 Dilution -R 1 .00000Acq Meth Set SC -AK102-AK103 Analysis_Lot_R SCRO1220814SampleWeightR 1 .00000Date Acquired 08/15/97 12 :02 : 30 PMPrep _Lot R XXX3104Initials WAAProcessing Method SCR AK102 AK103S_0122SSfj-r 3 R 100 .0000Surr 4 R 100 .0000DRO and RRO ResultsRet Time(min)Area(uV * sec)4Name1SURROGATE AK1022292367116 .010SURROGATE AK1033274903Diesel166 .789- i6 -.990 -- ---1968 16857809 .64229236797 .8844565 alpha AadrostPRODTC15 .763Sln Conc-20 .12397 554844988 .79020 .147327490130 .409Surr Rec _3(g )Surr Rec_4(g)TRUERRO_R4822 .00094822 .00094822 .000997 .8844822 .0009130 .4094822 .00094822 .0009True _Diesel_R7693 .63127693 .63127693 .63127693 .63127693 .631-j--7693 .6312Analysis Lot R : SCRO1220814SampleName ._ . LCSD 3120 Prep Lot R : XXX3115280 .00---260 .00- .240 .00--!220 .00 200 .00180 .00160 .00 .140 .00120 .00__100 .0080 .00 60 .00 _ -~N440 .00A20 .00~nnu1u0 .00 0 .005.010 .0015 .00Minutes20 .0025 .00Channel Descr . Rear_FIDSampleNameR LCSD 3120Acq Meth Set SC AK102 AK103Analysis_Lot R SCRO1220814Date Acquired 08/15/97 12 :39 :51 PMPrep-Lot-R XXX3115Processing Method SCR AK102 AK103S_0122 j7 -r 3 R 100 .0000Surr 4 R 100 .0000Dilution -R 1 .00000SampleWeightR 1 .00000Initials WAADRO and RRO Results0Name1SURROGATE AK102234Ret Time(min)SURROGATE AK103Diesel5 alpha Androst10 .99015 .767Area(uV*sec)Sln- Conc320619127 .221297627151 .580205348338148 .180320619107 .3435RRO20 .1276DTC98853305034 .54820 .1472976277C3622 .673118 .51791741Surr Rec_3Surr Rec_4TRUE RRO_R4882 .96798020 .95954882 .96798020 .95954882 .9679107 .3434882 .9679118 .517True Diesel R4882 .96794882 .96794882 .96798020 .95958020 .95958020 .95958020 .95958020 .9595. .na lys is Lot R : SCRO1220814SampleNameR .x74607001Prep_Lot_R : XXX311545 .0040 . 00 _35 .00_-130 .00-25 .00 -20 .0015 .00-10 .00-5 .00 -0 .00 ----5 .000.0~~~5 .0010 .0015 .00Minutes20 .0025 .00Channel Descr . Rear _ FIDSampleNameR 974607001Analysis Lot R SCRO1220814Acq Meth Set SC _AK102 _AK103Date Acquired 08/15/97 01 : 17 :12 PMPrep Lot R XXX3115Processing Method SCR _AK102 AK103S- 0122 j1 r_3_R 100 .0000Surr 4 R 100 .0000Dilution -R 1 .00000SampleWeightR 1 .00000Initials WAADRO and RRO ResultsName#1Ret Time(min)Area(uV*sec)Sln Conc-Surr Rec -3Surr Rec-4TRUE RRO R- -True Diesel R-SURROGATE AK10220949883 .128109 .7203- SURROGATE AK103213045108 .503103 .1786109 .7203103 .1786109 .7203103 .1786109 .7203103 .1786109 .7203103 .1786109 .7203103 .1786109 .7203103 .17863 Diesel15 .723469527186 .30745 alpha Androst15 .75320949870 .1405RRO19 .933428481218 .2236DTC20 .13321304584 .8367C3622 .663137270 .14084 .836-nalysis_Lot_R : SCRO1220814280 .00-_.260 .00-240 .00220 .00_-a140 .00_-~120 .00-1S ampleNameR .SB 8000 Prep Lot_R : XX X3115Channel Descr . Rear -FIDAcq Meth Set SC_AK102 AK103Date Acquired 08/15 / 97 02 :07 : 19 PMSampleName1 LSB 8000Dilution R 1 .00000Analysis Lot R SCRO1220814Prep_ Lot R XXX3115Processing Method SCR AK102 _AK103S_ 0122 AT r_3_R 0 .0000Surr 4 R 0 .0000SampleWeightR 1 .00000Initials WAADRO and RRO ResultsRet Time(min)Area(uV*sec)#Name1SURROGATE AK10319702SURROGATE AK1021 .00364 .3820688868642 .24203Diesel10 .99027 .33464 .38208642 .242045 alpha l-~ndrost218488728669 .57615 .7806888664 .38208642 .24205RRO18 .15723 .06364 .3820C2565 .3858642 .24206128383434138642 .2420718 .15764 .3820DTC20 .23764 .38208C3622 .66019708642 .242064 .38208642 .242083001Sln Conc-0 .784TRUERRO-R64 .3820TrueDiesel-R8642 .2420ialysis Lot R : S CRO122 0814eSampleNameR SR 5000 Prep Lot R :0814EB013280 .00 ._)260 .00240 .00-~220 .00--140 .00-120 .00___,'100 .0080 .00 -SnC460 .00 -NN40 .00 _~20 .00_11/I111I1I11III1I- - - - - - ' - - -V- - - - - - - - 1' - - - - - - A- - - - - - - - -I0 .000 .005.010 .0015 .00Minutes20 .0025 .00Channel Descr . Rear _ FID SampleNameR LSR 5000 Dilution R 1 .00000Acq Meth Set SC _AK102 AK103 Analysis Lot R SCRO1220814 SampleWeightR 1 .00000Date Acquired 08/15/97 02 :44 :34 PM Prep Lot R 0814EB01 Initials WAAProcessing Method SCR AK102 AK103S-01225M'tr 3 R 0 .0000Surr 4 R 0 .0000DRO and RRO ResultsRet Time(min)Area(uV* sec)#Name1SURROGATE AK102222342SURROGATE AK-1038 .865814 .91343Diesel998155240 .146620760685240 .14665 alpha Androst18 . 22715921487 .480814 .9134C25223425240 .1466515 .790823 .779814 .9134415 .70050 .8355240 .1466814 .91346RRODTC10388838814 .9134720 .0375240 .146620 .17399815Sln Conc-TRUE-RRO-R5290 .9825240 .146639 .7475240 .1466TrueDiesel-R814 .9134814 .9134Semi-Volatiles Sample QC SummaryCT&E Environmental ServicesQA/QC Data De liverablesWorkorder Number :a- . 4&Analysis :Method :8081Matrix :c-(Polychlorinated BiphenylsEPALiquidAnalysis :Analysis Lot Number : W02-34[!.XaExtraction Lot Number:)C)(X 31( DAcceptance Criteria :Assurance Notes:Yes No N/AA . Holding Time :All criteria met .XEE1All criteria met.ElAll criteria met.13 . Surrogates :C . Notes :All criteria met.®aQZ F114 days from sample collection forTCLP extraction .7 days from sample collection (orTCLP extraction ) for prep extraction.40 days from extraction for analysis.10% - 87% Recovery for Tetra or59% - 122% Recovery for Deca./ certify that except as specifically noted in this report, all statements and data appearing in this report are in conformancewith the provisions of the Quality Assurance Plan (QAP) prepared by this firm and on file with the Al9skp Department ofEanvironmental Conservation .Analyst's Signature :Reviewer 's Signature :Printed Name & Date Lizhen ZhangPrinted Name & Date:Semi -Volatiles Quality Control Summary PageCT&E Environmental Services . Inc .QA/QC Data DeliverablesAnalysis Date :$ llt_lq_Analysis :Polychlorinated Biphenyls-2Analysis Lot , Number : SzRv7 3 4144Extraction Lot Number :X x X 3 l 10Method : EPA 8081LiquidMatrix :Acceptance Criteria :Assurance Notes:Analysis:Yes No'RA2 >0 .99A . Calibration :All criteria met .®F7B . Method Blank :All criteria met.®0C . Continuing Calibration Verification Std :All criteria met .©F7D . Laboratory Control Sample :All criteria met.0050% - 139% Recovery for Aroclor 124244% - 116% Recovery for Aroclor 125439%- 110% Recovery for Aroclor 1260E . Laboratory Control Sample Duplicate :All criteria met.®Q50% - 139% Recovery for Aroclor 12420±25% Relative Percent DifferenceAll criteria met.All criteria met.F. QC Surrogates:G . Notes :®a Greater ThanACZACZ Laboratories , Steamboat, COAELF American Environmental Laboratories , Pensacola, FLAENP American Environmental Network , Portland, ORALTC Alta Analytical Lab Incorporated, El Dorado Hills, CAAPPL Agriculture & Priority Pollutants Laboratories , Fresno, CAARDL Applied Research and Development Lab, Inc ., (ARDL) Mt . Vernon, ILARI Analytical Resources , Inc ., Seattle, WAATCA Analytica, Anchorage, AKATCC Analytica, COATIA Analytical Technologies, Inc ., Anchorage, AKATIR Analytical Technologies, Inc ., Renton, WAATIS Analytical Technologies, Inc ., San Diego, CAATOX Air Toxics LTD, Folsom, CABCLB BC Laboratories, Bakersfield, CABD Blank Spike DuplicateBoreochem Mobile Lab & Analytical ServicesBMLABRS Brelje & Race , Santa Rosa, CABS Blank SpikeCASA Columbia Analytical Services , Inc., Anchorage, AKCASB Columbia Analytical Services, Inc ., Bothell, WACASK Columbia Analytical Services, Inc ., Kelso, WACC Continuing Calibration VerificationCCAC Coast-to-Coast Analytical Services, Inc ., Camarillo, CACCSJ Coast-to-Coast Analytical Services , Inc., San Jose, CACDMCDM Federal Programs CorporationCHEM Chemic Laboratory, San Diego, CACKY CKY Inc ., Torrance, CACLPA Contract Laboratory Program Accuracy Limits for Spiked SamplesCLPCC CLP Continuing Calibration Acceptance CriteriaCLPIC CLP Initial Calibration Acceptance CriteriaCLPLR Contract Laboratory Program Precision for Lab ReplicatesCLPP Contract Laboratory Program Precision Limits for Spiked SamplesCLTP Clayton Environmental Consultants, Inc ., Pleasanton, CACS Client SampleCTB Curtis & Tompkins, Berkeley, CACTE CT&E Environmental Services, Inc ., Anchorage, AKCTEC CT&E Environmental Services, Inc ., Charleston, NCDDL Method Defined Detection LimitDMP D & M Laboratories, Petaluma, CADOWL Dowl Engineering Alaska Test Labs, Anchorage, AKEBAEBAECEN Ecology & Environment, Inc .ECI EcoChem, Inc .EQL Estimated Quantitation LimitETCS ETC, Santa Rosa, CAFORA Forensic AnalyticalIC Initial Calibration VerificationCodeNameIDL Instrument Detection LimitIN Internal StandardKDKnown ( External Reference Material ) DuplicateLAB1 Laboratory 1LAB2 Laboratory 2LAL Lockheed Analytical Laboratory , Las Vegas, NVLASLAS Laboratories, Inc .LB Lab BlankLCC Laboratory Continuing Calibration AccuracyLDC Laboratory Data ConsultantsLIC Laboratory Initial Calibration AccuracyLLD Lowest Level of Detection _LLR Laboratory Established Precision for Lab ReplicatesLR Lab ReplicateLSA Laboratory Sample Accuracy for Spiked SamplesLSP Laboratory Sample Precision for Spiked SamplesLTL Laucks Testing Lab, Inc .MASA MultiChem Analytical Services , Anchorage, AKMASR MultiChem Analytical Services , Renton, WAMDL Method Detection LimitMEA Method Established Accuracy for Spiked SamplesMECC Method Established Continuing Calibration Acceptance CriteriaMEIC Method Established Initial Calibration Acceptance CriteriaMELR Method Established Precision for Laboratory ReplicatesMEP Method Established Precision for Spiked SamplesMLR Matrix Laboratory Replicate PrecisionMSGC/MS Result - Value Confirmed Using GC/MSMS Lab Matrix SpikeMSA Matrix Spike Accuracy for Spiked SamplesMSP Matrix Spike Precision for Spiked SamplesMSSL Mountain States Analytical , Salt Lake City, UTNA Not ApplicableNA Not Available - Result Not AvailableNC Non-Client SampleNCAB North Creek Analytical , Bothell, WANCAP North Creek Analytical , Beaverton, ORND Not DetectedNETB NET Burbank, Burbank, CANETC NET Cambridge , Bedford, MANET Portland, Portland, ORNETONETS NET Pacific , Inc., Santa Rosa, CANR Not Reported - Data Not Reported .NTL Northern Testing Laboratories , Anchorage, AKNU Not Usable - Data Not UsableOEIR OnSite Environmental , Inc ., Redmond, WAPAC Pacific Analytical , Carlsbad, CAPARA Paragon Analytics, Inc ., COPHLE Philip EnvironmentalPIC Pace Analytical Services , Inc ., Camarillo, CAPIHB Pace Analytical Services , Inc ., Huntington Beach, CAPIL Pace Analytical Services , Inc., Lenexa, KSPIM Pace Analytical Services , Inc ., Minneapolis, MNPIN Pace Analytical Services , Inc ., Novato, CAPINY Pace Analytical Services , Inc ., New York, NYPIP Pace Analytical Services , Inc ., Pittsburgh, PACode NamePITS Pace Analytical Services, Inc ., Tampa Bay, FLPIWF Pace Analytical Services, Inc ., Wappingers Falls, NYPQL Practical Quantitation LimitPR Primary Result - The Primary Result for a ParameterPRL Parameter Range LimitQALA Quality Analytical Laboratores, Inc ., Montgomery, ALQALC Quality Analytical Laboratories, Inc., Redding, CAQES Quanterra Environmental Services, Santa Ana, CAQESA Quanterra Environmental Services, Arvada, COQuanterra Environmental Services, North Canton, OHQESCQESF Quanterra Environmental Services, Tampa, FLQESG Quanterra Environmental Services, Garden Grove,QESI Quanterra Environmental Services, City of Industry, CAQESJ Quanterra - Research Triangle Park Lab ., Raleigh, NCQESK Quanterra Environmental Services, Knoxville, TNQESL Quanterra Environmental Services, St . Louis, MOQESN Quanterra Environmental Services, Anchorage, AKQESP Quanterra Environmental Services, Pittsburg, PAQESR Quanterra Environmental Services, Richland, WAQESS Quanterra Environmental Services, Sacramento, CAQEST Quanterra Environmental Services, Austin, TXQESZ Quanterra Environmental Services, Anchorage, AKRM Known (External Reference Material)RS Reagent SolventSAS Sound Analytical Services, Inc ., Tacoma, WASBSA Both Reagent and Matrix Sample Accuracy for SurrogatesSBSP Both Reagent and Matrix Sample Precision for SurrogatesSC3S S-Cubed, A Division of Maxwell Laboratories , Inc ., San Diego, CASCLA Contract Laboratory Program Limits for Surrogate AccuracySCLP Contract Laboratory Program Limits for Surrogate PrecisionSD Lab Matrix Spike DuplicateSLSA Laboratory Sample Limits for Accuracy for SurrogatesSLSP Laboratory Sample Limits for Precision for SurrogatesMethod Established Limits for Accuracy for SurrogatesSMEASMEP Method Established Limits for Precision for SurrogatesSMSA Sample Matrix Limits for Accuracy for SurrogatesSMSP Sample Matrix Limits for Precision for SurrogatesSPEC Spectra Laboratory, Inc ., Tacoma, WAStandard Reference Accuracy Defined by Agency/ ManufacturerSRADSRMA Standard Reference Material Accuracy Limits Determined by LabSRMP Standard Reference Material Precision Limits Determined by LabSRPDStandard Reference Precision Defined by Agency /ManufacturerSU SurrogateSWAG Shannon & Wilson, Inc ., Anchorage, AKSWLB Southwest LaboratorySWRI Southwest Resarch Institute, San Antonio, TXTI Tentatively Identified CompoundTRID Triangle Laboratories, Inc ., Durham, NCti11CT&E Environmental Services Inc .D Laboratory DivisionLaboratory Analysis ReportAugust 15, 1997Victor HarrisMontgomery Watson Americas Inc4100 Spenard RdAnchorage, AK 99517-2901Client NameMontgomery Watson Americas IncProject ID COE-Gambell-New Well [9740761PrintedAugust 15, 1997Enclosed are the analytical results associated with the above project.As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Programis maintained by CT&E. A copy of our Quality Control Manual that outlines this program is availableat your request.Except as specifically noted, all statements and data in this report are in conformance to theprovisions set forth in our Quality Assurance Program Plan.If you have any questions regard this report or if we can be of any other assistance, please callyour CT&E Project Manager at (9n 562-2343 .The following descriptors may be found on your report which will serve to further qualify the data .U - Indicates the compound was analyzed for but not detected.J - Indicates an estimated value that falls below PQL, but is greater than the MDL.B - Indicates the analyte is found in the blank associated with the sample.* - The analyte has exceeded allowable limits .GT - Greater ThanD - Secondary DilutiomLT - Less Thaw- Surrogate out of rangy200 W . Potter Drive, Anchorag.. AK 99618-1606 - Tel: (907) 562-2343 Fax : (907) 561-53013180 Pager Road, Fairbanks, AK 99709-6471 - Tel: (907) 474-8658 Fax: (907) 474-9685ENVIRONMENTAL FACILITIES IN ALASKA . CALIFORNIA, FLORIDA . ILLINOIS, MARYLAND, MICHIGAN. MISSOURI. NEW JERSEY, OHIO, WEST VIRGINIACT&E Environmental Services Inc .CT&E Ref .# 974076001Montgomery Watson Americas IncClient NameCOE-Gambell-New WellProject Name/#Client PO# 605Printed Date/Time08/15/97 17 :26Collected Date/Time 07/24/97 08 :00Received DateJTime 07/28/97 08 :35Technical Director: Stephen C . EdeClient Sample ID 97GAM001 NVWMatrixOrdered ByWater ( Surface, Eff., Ground)PWSIDReleased By It`sample Remarks :ParameterResultsPQLUnits MethodAllowable Prop AnalysisLimitsDateDatelnitAK102Dirsel Range Organics0 .1240 .101 mg/L77 .1%AK102 DRO07/29/9T 07/30/97 WAASurrogates5a Androstane csurr>AK102 DRO (50-150) 07/29/97 07/30/97Semi-Volatiles Sample QC Summary PageCT&E Environmental Services Inc..QA/QC Data DeliverablesWorkorder Number :SCRotZZO73 0xPc 30{Extraction Lot Number :vu x(* 7t(57LAnalysis : Diesel Range OrganicsMethod : AKI02Matrix :Analysis Lot Number :LiquidAnalysis :Assurance Notes : Acceptance Criteria :Yes No N/AA . Holding rime :All criteria met.All criteria met.All criteria met.B . Surrogates :Allcriteriamet.014 days from sample collection forTCLP extraction .7 days from sample collection (orTCLP extraction) for prep extraction .40 days from extraction (orcollection time if oil) for analysis.50% - 150% RecoveryC . Notes :I certify that except as speeiftcallv notedin this report, all statements and data appearing in this report are in conformancewith the provisions of the Quality Assurance Plan (QAP) prepared by this firm and on file with the Alaska Department ofEnvironmental Conservation.Analyst' s Signature :Reviewer's Signature :- -Printed Name & Date :Printed Name & Date :Semi-Volatiies Quality Contro l Summary Page.Cf&E Environmental Services Inc .QAIQC Data . . Deliverables- 3,0 - 47Analysis Date :Analysis :Method :Matrix :Analysis Lot Number:Extraction Lot Number:Diesel Range OrganicsAK102LiquidAssurance Notes :Analysis :SCRo' tLo7;~Yx/3d a8Acceptance Criteria :Yes NoA . Calibration :All criteria met.ME]Correlation Coefficient >/=0 .995,Relative Standard Deviation